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Easy Preparation of [Bis(trifluoroacetoxy)iodo]arenes from Iodoarenes, with Sodium Percarbonate as the Oxidant†
Easy and effective preparations of the nearly pure [bis(trifluoroacetoxy)-iodo]arenes, ArI(OCOCF)(3), from some iodoarenes, ArI, are reported, using an anhydrous sodium percarbonate/(CF(3)CO)(2)O/CH(2)Cl(2) system. The colorless, freshly prepared ArI(OCOCF(3))(2) thus obtained were 98-99% pure (by i...
Autores principales: | , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2002
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6146490/ http://dx.doi.org/10.3390/71100810 |