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Chemical Fingerprint and Multicomponent Quantitative Analysis for the Quality Evaluation of Cyclocarya paliurus Leaves by HPLC–Q–TOF–MS

Cyclocarya paliurus is an edible and medicinal plant containing various bioactive components with significant health benefits. A combinative method using high-performance liquid chromatography (HPLC) fingerprint and quantitative analysis was developed and successfully applied for characterization an...

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Autores principales: Cao, Yanni, Fang, Shengzuo, Yin, Zhiqi, Fu, Xiangxiang, Shang, Xulan, Yang, Wanxia, Yang, Huimin
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2017
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6150387/
https://www.ncbi.nlm.nih.gov/pubmed/29112173
http://dx.doi.org/10.3390/molecules22111927
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author Cao, Yanni
Fang, Shengzuo
Yin, Zhiqi
Fu, Xiangxiang
Shang, Xulan
Yang, Wanxia
Yang, Huimin
author_facet Cao, Yanni
Fang, Shengzuo
Yin, Zhiqi
Fu, Xiangxiang
Shang, Xulan
Yang, Wanxia
Yang, Huimin
author_sort Cao, Yanni
collection PubMed
description Cyclocarya paliurus is an edible and medicinal plant containing various bioactive components with significant health benefits. A combinative method using high-performance liquid chromatography (HPLC) fingerprint and quantitative analysis was developed and successfully applied for characterization and quality evaluation of C. paliurus leaves collected from 18 geographical locations of China. For the fingerprint analysis, 21 common peaks were observed among the 18 samples, and these peaks were identified by high-performance liquid chromatography coupled with quadrupole time-of-flight mass spectrometry (HPLC–Q–TOF–MS), while a simultaneous quantification of 16 markers was conducted to interpret the variations of contents of these bioactive compounds among the C. paliurus leaves from different geographical locations. Quantification results showed that the contents of these sixteen investigated compounds varied greatly among the leaves from different locations. The developed new method would be a valuable reference for further study and development of this bioactive plant.
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spelling pubmed-61503872018-11-13 Chemical Fingerprint and Multicomponent Quantitative Analysis for the Quality Evaluation of Cyclocarya paliurus Leaves by HPLC–Q–TOF–MS Cao, Yanni Fang, Shengzuo Yin, Zhiqi Fu, Xiangxiang Shang, Xulan Yang, Wanxia Yang, Huimin Molecules Article Cyclocarya paliurus is an edible and medicinal plant containing various bioactive components with significant health benefits. A combinative method using high-performance liquid chromatography (HPLC) fingerprint and quantitative analysis was developed and successfully applied for characterization and quality evaluation of C. paliurus leaves collected from 18 geographical locations of China. For the fingerprint analysis, 21 common peaks were observed among the 18 samples, and these peaks were identified by high-performance liquid chromatography coupled with quadrupole time-of-flight mass spectrometry (HPLC–Q–TOF–MS), while a simultaneous quantification of 16 markers was conducted to interpret the variations of contents of these bioactive compounds among the C. paliurus leaves from different geographical locations. Quantification results showed that the contents of these sixteen investigated compounds varied greatly among the leaves from different locations. The developed new method would be a valuable reference for further study and development of this bioactive plant. MDPI 2017-11-07 /pmc/articles/PMC6150387/ /pubmed/29112173 http://dx.doi.org/10.3390/molecules22111927 Text en © 2017 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Cao, Yanni
Fang, Shengzuo
Yin, Zhiqi
Fu, Xiangxiang
Shang, Xulan
Yang, Wanxia
Yang, Huimin
Chemical Fingerprint and Multicomponent Quantitative Analysis for the Quality Evaluation of Cyclocarya paliurus Leaves by HPLC–Q–TOF–MS
title Chemical Fingerprint and Multicomponent Quantitative Analysis for the Quality Evaluation of Cyclocarya paliurus Leaves by HPLC–Q–TOF–MS
title_full Chemical Fingerprint and Multicomponent Quantitative Analysis for the Quality Evaluation of Cyclocarya paliurus Leaves by HPLC–Q–TOF–MS
title_fullStr Chemical Fingerprint and Multicomponent Quantitative Analysis for the Quality Evaluation of Cyclocarya paliurus Leaves by HPLC–Q–TOF–MS
title_full_unstemmed Chemical Fingerprint and Multicomponent Quantitative Analysis for the Quality Evaluation of Cyclocarya paliurus Leaves by HPLC–Q–TOF–MS
title_short Chemical Fingerprint and Multicomponent Quantitative Analysis for the Quality Evaluation of Cyclocarya paliurus Leaves by HPLC–Q–TOF–MS
title_sort chemical fingerprint and multicomponent quantitative analysis for the quality evaluation of cyclocarya paliurus leaves by hplc–q–tof–ms
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6150387/
https://www.ncbi.nlm.nih.gov/pubmed/29112173
http://dx.doi.org/10.3390/molecules22111927
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