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Analytical methods for determination of bisphenol A, 4-tert-octylphenol and 4-nonylphenol in herrings and physiological fluids of the grey seal
• The aim of this work was to develop the methods of determination for phenol derivatives: bisphenol A (BPA), 4-tert-octylphenol (OP) and 4-nonylphenol (NP), in the whole body of herring Clupea harengus and in physiological fluids of the Baltic grey seal Halichoerus grypus grypus (blood and milk). •...
Autores principales: | , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Elsevier
2018
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6168930/ https://www.ncbi.nlm.nih.gov/pubmed/30294560 http://dx.doi.org/10.1016/j.mex.2018.09.007 |
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author | Staniszewska, Marta Nehring, Iga Falkowska, Lucyna Bodziach, Karina |
author_facet | Staniszewska, Marta Nehring, Iga Falkowska, Lucyna Bodziach, Karina |
author_sort | Staniszewska, Marta |
collection | PubMed |
description | • The aim of this work was to develop the methods of determination for phenol derivatives: bisphenol A (BPA), 4-tert-octylphenol (OP) and 4-nonylphenol (NP), in the whole body of herring Clupea harengus and in physiological fluids of the Baltic grey seal Halichoerus grypus grypus (blood and milk). • Methods were based on liquid chromatography coupled with a fluorescence detector (HPLC-FL). • These methods were satisfactorily validated, each showing good recovery (>80%) and precision (RSD < 15%). Regarding the limit of quantification (LOQ), this was established at <2 ng g(−1) for herring, <0.07 ng cm(-3) for blood and <0.1 ng cm(−3) for milk. |
format | Online Article Text |
id | pubmed-6168930 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2018 |
publisher | Elsevier |
record_format | MEDLINE/PubMed |
spelling | pubmed-61689302018-10-05 Analytical methods for determination of bisphenol A, 4-tert-octylphenol and 4-nonylphenol in herrings and physiological fluids of the grey seal Staniszewska, Marta Nehring, Iga Falkowska, Lucyna Bodziach, Karina MethodsX Environmental Science • The aim of this work was to develop the methods of determination for phenol derivatives: bisphenol A (BPA), 4-tert-octylphenol (OP) and 4-nonylphenol (NP), in the whole body of herring Clupea harengus and in physiological fluids of the Baltic grey seal Halichoerus grypus grypus (blood and milk). • Methods were based on liquid chromatography coupled with a fluorescence detector (HPLC-FL). • These methods were satisfactorily validated, each showing good recovery (>80%) and precision (RSD < 15%). Regarding the limit of quantification (LOQ), this was established at <2 ng g(−1) for herring, <0.07 ng cm(-3) for blood and <0.1 ng cm(−3) for milk. Elsevier 2018-09-21 /pmc/articles/PMC6168930/ /pubmed/30294560 http://dx.doi.org/10.1016/j.mex.2018.09.007 Text en © 2018 The Authors http://creativecommons.org/licenses/by/4.0/ This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Environmental Science Staniszewska, Marta Nehring, Iga Falkowska, Lucyna Bodziach, Karina Analytical methods for determination of bisphenol A, 4-tert-octylphenol and 4-nonylphenol in herrings and physiological fluids of the grey seal |
title | Analytical methods for determination of bisphenol A, 4-tert-octylphenol and 4-nonylphenol in herrings and physiological fluids of the grey seal |
title_full | Analytical methods for determination of bisphenol A, 4-tert-octylphenol and 4-nonylphenol in herrings and physiological fluids of the grey seal |
title_fullStr | Analytical methods for determination of bisphenol A, 4-tert-octylphenol and 4-nonylphenol in herrings and physiological fluids of the grey seal |
title_full_unstemmed | Analytical methods for determination of bisphenol A, 4-tert-octylphenol and 4-nonylphenol in herrings and physiological fluids of the grey seal |
title_short | Analytical methods for determination of bisphenol A, 4-tert-octylphenol and 4-nonylphenol in herrings and physiological fluids of the grey seal |
title_sort | analytical methods for determination of bisphenol a, 4-tert-octylphenol and 4-nonylphenol in herrings and physiological fluids of the grey seal |
topic | Environmental Science |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6168930/ https://www.ncbi.nlm.nih.gov/pubmed/30294560 http://dx.doi.org/10.1016/j.mex.2018.09.007 |
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