The Synthesis of Unsubstituted Cyclic Imides Using Hydroxylamine under Microwave Irradiation†

Unsubstituted cyclic imides were synthesized from a series of cyclic anhydrides, hydroxylamine hydrochloride (NH(2)OH∙HCl), and 4-N,N-dimethylamino-pyridine (DMAP, base catalyst) under microwave irradiation in monomode and multimode microwaves. This novel microwave synthesis produced high yields of...

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Detalles Bibliográficos
Autores principales: Benjamin, Ellis, Hijji, Yousef
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2008
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6245478/
https://www.ncbi.nlm.nih.gov/pubmed/18259138
http://dx.doi.org/10.3390/molecules13010157
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author Benjamin, Ellis
Hijji, Yousef
author_facet Benjamin, Ellis
Hijji, Yousef
author_sort Benjamin, Ellis
collection PubMed
description Unsubstituted cyclic imides were synthesized from a series of cyclic anhydrides, hydroxylamine hydrochloride (NH(2)OH∙HCl), and 4-N,N-dimethylamino-pyridine (DMAP, base catalyst) under microwave irradiation in monomode and multimode microwaves. This novel microwave synthesis produced high yields of the unsubstituted cyclic imides for both the monomode (61 - 81%) and multimode (84 - 97%) microwaves.
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spelling pubmed-62454782018-11-26 The Synthesis of Unsubstituted Cyclic Imides Using Hydroxylamine under Microwave Irradiation† Benjamin, Ellis Hijji, Yousef Molecules Article Unsubstituted cyclic imides were synthesized from a series of cyclic anhydrides, hydroxylamine hydrochloride (NH(2)OH∙HCl), and 4-N,N-dimethylamino-pyridine (DMAP, base catalyst) under microwave irradiation in monomode and multimode microwaves. This novel microwave synthesis produced high yields of the unsubstituted cyclic imides for both the monomode (61 - 81%) and multimode (84 - 97%) microwaves. MDPI 2008-01-25 /pmc/articles/PMC6245478/ /pubmed/18259138 http://dx.doi.org/10.3390/molecules13010157 Text en © 2008 by MDPI (http://www.mdpi.org). Reproduction is permitted for noncommercial purposes.
spellingShingle Article
Benjamin, Ellis
Hijji, Yousef
The Synthesis of Unsubstituted Cyclic Imides Using Hydroxylamine under Microwave Irradiation†
title The Synthesis of Unsubstituted Cyclic Imides Using Hydroxylamine under Microwave Irradiation†
title_full The Synthesis of Unsubstituted Cyclic Imides Using Hydroxylamine under Microwave Irradiation†
title_fullStr The Synthesis of Unsubstituted Cyclic Imides Using Hydroxylamine under Microwave Irradiation†
title_full_unstemmed The Synthesis of Unsubstituted Cyclic Imides Using Hydroxylamine under Microwave Irradiation†
title_short The Synthesis of Unsubstituted Cyclic Imides Using Hydroxylamine under Microwave Irradiation†
title_sort synthesis of unsubstituted cyclic imides using hydroxylamine under microwave irradiation†
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6245478/
https://www.ncbi.nlm.nih.gov/pubmed/18259138
http://dx.doi.org/10.3390/molecules13010157
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