Cargando…

Copper(II) Sulfamate: An Efficient Catalyst for the One-Pot Synthesis of 3,4-Dihydropyrimidine-2(1H)-ones and thiones

A simple, efficient procedure for the one-pot Biginelli condensation reaction of aldehydes, β-ketoesters and urea or thiourea employing copper(II) sulfamate as a novel catalyst is described. Compared to the classical Biginelli reaction conditions, the present method has the advantages of good yields...

Descripción completa

Detalles Bibliográficos
Autores principales:	Liu, Chen-Jiang, Wang, Ji-De
Formato:	Online Artículo Texto
Lenguaje:	English
Publicado:	Molecular Diversity Preservation International 2009
Materias:	Article
Acceso en línea:	https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6254017/ https://www.ncbi.nlm.nih.gov/pubmed/19223824 http://dx.doi.org/10.3390/molecules14020763

Ejemplares similares

Three Component Reaction: An Efficient Synthesis and Reactions of 3,4-Dihydropyrimidin-2(1H)-Ones and Thiones Using New Natural Catalyst
por: Elmaghraby, A. M., et al.
Publicado: (2013)

Efficient One-Pot Synthesis of 3,4-Dihydropyrimidin-2(1H)-ones via a Three-Component Biginelli Reaction
por: Bosica, Giovanna, et al.
Publicado: (2021)

An Efficient One-Pot Protocol for the Synthesis of Substituted 3,4-Dihydropyrimidin-2(1H)-ones Using Metallophthalocyanines (MPcs) as Potent Heterogeneous Catalysts: Synthesis, Characterization, Aggregation and Antimicrobial Activity
por: Hamdi, Naceur, et al.
Publicado: (2017)

Sulfamic acid pyromellitic diamide-functionalized MCM-41 as a multifunctional hybrid catalyst for melting-assisted solvent-free synthesis of bioactive 3,4-dihydropyrimidin-2-(1H)-ones
por: Valiey, Ehsan, et al.
Publicado: (2021)

Synthesis of 3,4-Dihydropyrimidin-2(1H)-Ones and Their Corresponding 2(1H)Thiones Using Trichloroacetic Acid as a Catalyst under Solvent-Free Conditions
por: Karimi-Jaberi, Zahed, et al.
Publicado: (2012)

Pumice as a Novel Natural Heterogeneous Catalyst for the Designation of 3,4-Dihydropyrimidine-2-(1H)-ones/thiones under Solvent-Free Conditions
por: El-Lateef, Hany M. Abd, et al.
Publicado: (2022)

Efficient and Recoverable Bio-Organic Catalyst Cysteine for Synthesis, Docking Study, and Antifungal Activity of New Bio-Active 3,4-Dihydropyrimidin-2(1H)-ones/thiones Under Microwave Irradiation
por: Elkanzi, Nadia A. A., et al.
Publicado: (2022)

An Efficient Synthesis of 3,4-Dihydropyrimidin-2(1H)-Ones and Thiones Catalyzed by a Novel Brønsted Acidic Ionic Liquid under Solvent-Free Conditions
por: Zhang, Yonghong, et al.
Publicado: (2015)

An Efficient, Eco-friendly and Sustainable One-Pot Synthesis of 3,4-Dihydropyrimidin-2(1H)-ones Directly from Alcohols Catalyzed by Heteropolyanion-Based Ionic Liquids
por: Fu, Renzhong, et al.
Publicado: (2017)

Zeolite catalyzed solvent-free one-pot synthesis of dihydropyrimidin-2(1H)-ones – A practical synthesis of monastrol
por: Kulkarni, Mukund G, et al.
Publicado: (2009)

Ammonium Trifluoroacetate-Mediated Synthesis of 3,4-dihydropyrimidin-2(1H)-ones
por: Raju, Chandran, et al.
Publicado: (2011)

An Efficient One-Pot Green Protocol for the Synthesis of 5-Unsubstituted 3,4-Dihydropyrimidin-2(1H)-Ones Using Recyclable Amberlyst 15 DRY as a Heterogeneous Catalyst via Three-Component Biginelli-Like Reaction
por: Jetti, Srinivasa Rao, et al.
Publicado: (2012)

Electrolytic copper as cheap and effective catalyst for one-pot triazole synthesis
por: Mularski, Jacek, et al.
Publicado: (2018)

One-pot synthesis of 3,4-dihydropyrimidin-2(1H)-ones catalyzed by SO(3)H@imineZCMNPs as a novel, efficient and reusable acidic nanocatalyst under solvent-free conditions
por: Abbaspour-Gilandeh, Esmayeel, et al.
Publicado: (2018)

Aerobic copper-promoted oxidative dehydrosulfurative carbon–oxygen cross-coupling of 3,4-dihydropyrimidine-1H-2-thiones with alcohols
por: Lee, Jihong, et al.
Publicado: (2021)

Silica: An efficient catalyst for one-pot regioselective synthesis of dithioethers
por: Kundu, Samir, et al.
Publicado: (2014)

One Pot Synthesis of Copper Oxide Nanoparticles for Efficient Antibacterial Activity
por: Rajamohan, Rajaram, et al.
Publicado: (2022)

Tungsten-substituted molybdophosphoric acid impregnated with kaolin: effective catalysts for the synthesis of 3,4-dihydropyrimidin-2(1H)-ones via biginelli reaction
por: Aher, Dipak S., et al.
Publicado: (2021)

Synthesis of 3,4-Dihydropyrimidin(thio)one Containing Scaffold: Biginelli-like Reactions
por: Sánchez-Sancho, Francisco, et al.
Publicado: (2022)

A facile hydrothermal synthesis of high-efficient NiO nanocatalyst for preparation of 3,4-dihydropyrimidin-2(1H)-ones
por: Khashaei, Maryam, et al.
Publicado: (2022)

Efficient one-pot synthesis and dehydrogenation of tricyclic dihydropyrimidines catalyzed by OMS-2-SO(3)H, and application of the functional-chromophore products as colorimetric chemosensors
por: Mardazad, Neda, et al.
Publicado: (2021)

Recyclable photocatalyst perovskite as a single-electron redox mediator for visible-light-driven photocatalysis gram-scale synthesis of 3,4-dihydropyrimidin-2-(1H)-ones/thiones in air atmosphere
por: Mohamadpour, Farzaneh
Publicado: (2023)

Visible-Light-Induced Radical Condensation Cyclization to Synthesize 3,4-Dihydropyrimidin-2-(1H)-ones/thiones Using Photoexcited Na(2) Eosin Y as a Direct Hydrogen Atom Transfer (HAT) Catalyst
por: Mohamadpour, Farzaneh
Publicado: (2022)

Targeting Cancer Stem Cells with Novel 4-(4-Substituted phenyl)-5-(3,4,5-trimethoxy/3,4-dimethoxy)-benzoyl-3,4-dihydropyrimidine-2(1H)-one/thiones
por: Bhat, Mashooq Ahmad, et al.
Publicado: (2016)

Sulfamic acid promoted one-pot multicomponent reaction: a facile synthesis of 4-oxo-tetrahydroindoles under ball milling conditions
por: Lambat, Trimurti L., et al.
Publicado: (2019)

Fe(III)-montmorillonite catalysed one pot synthesis of 5-substituted dihydropyrimidine derivatives as potent antimicrobial agents
por: B.M., Vinoda, et al.
Publicado: (2016)

Synthesis of structurally diverse 3,4-dihydropyrimidin-2(1H)-ones via sequential Biginelli and Passerini reactions
por: Boukis, Andreas C, et al.
Publicado: (2017)

Synthesis, Characterization, and Anticancer Activities Evaluation of Compounds Derived from 3,4-Dihydropyrimidin-2(1H)-one
por: Liu, Ye, et al.
Publicado: (2019)

Antimicrobial evaluation of some novel derivatives of 3,4-dihydropyrimidine-2(1H)-one
por: Jalali, M., et al.
Publicado: (2012)

Copper-Promoted One-Pot Approach: Synthesis of Benzimidazoles
por: Boddapati, S. N. Murthy, et al.
Publicado: (2020)

A green protocol for the one-pot synthesis of 3,4-disubstituted isoxazole-5(4H)-ones using modified β-cyclodextrin as a catalyst
por: Tajbakhsh, Mahdieh, et al.
Publicado: (2022)

New Efficient Synthesis of 3,4-Dihydropyrimidin-2(1H)-ones Catalyzed by Benzotriazolium-Based Ionic Liquids under Solvent-Free Conditions
por: Liu, Zhiqing, et al.
Publicado: (2016)

Dataset on Insilico approaches for 3,4-dihydropyrimidin-2(1H)-one urea derivatives as efficient Staphylococcus aureus inhibitor
por: Oyebamiji, Abel Kolawole, et al.
Publicado: (2020)

Retraction: Boric acid in magnetized water: clean and powerful media for synthesis of 3,4-dihydropyrimidin-2(1H)-ones
por: Khakyzadeh, Vahid, et al.
Publicado: (2021)

A Green, Expeditious, One-Pot Synthesis of 3, 4-Dihydropyrimidin-2(1H)-ones Using a Mixture of Phosphorus Pentoxide-Methanesulfonic Acid at Ambient Temperature
por: Borse, Amulrao, et al.
Publicado: (2012)

Titania Nanotubes-Bonded Sulfamic Acid as an Efficient Heterogeneous Catalyst for the Synthesis of n-Butyl Levulinate
por: Zhou, Shuolin, et al.
Publicado: (2022)

1-(3-Fluorophenyl)-4,4,6-trimethyl-3,4-dihydropyrimidine-2(1H)-thione
por: Yamin, Bohari M., et al.
Publicado: (2011)

4,4,6-Trimethyl-1-(3-methylphenyl)-3,4-dihydropyrimidine-2(1H)-thione
por: Saeed, Aamer, et al.
Publicado: (2010)

1-(4-Chlorophenyl)-4,4,6-trimethyl-3,4-dihydropyrimidine-2(1H)-thione
por: Saeed, Aamer, et al.
Publicado: (2010)

5-Acetyl-4-(4-methoxyphenyl)-6-methyl-3,4-dihydropyrimidine-2(1H)-thione
por: Anuradha, N., et al.
Publicado: (2009)

Cannot write session to /tmp/vufind_sessions/sess_ppkfa51hbsjet5petfuhtuol4j