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The Reaction of Diethyl Bromomalonate with p-tert-Butylthia-calix[4]arene: An Approach to Asymmetrical Derivatives
New dissymmetric and asymmetric p-tert-butylthiacalix[4]arene derivatives were prepared as a result of the reaction of p-tert-butylthiacalix[4]arene with diethyl bromomalonate in the presence of different alkali metals (Cs, K and Na) in refluxing acetone for 7 days. The structures of the prepared co...
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Molecular Diversity Preservation International
2009
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Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6254204/ https://www.ncbi.nlm.nih.gov/pubmed/19471195 http://dx.doi.org/10.3390/molecules14051755 |
Sumario: | New dissymmetric and asymmetric p-tert-butylthiacalix[4]arene derivatives were prepared as a result of the reaction of p-tert-butylthiacalix[4]arene with diethyl bromomalonate in the presence of different alkali metals (Cs, K and Na) in refluxing acetone for 7 days. The structures of the prepared compounds were investigated by IR, (1)H-NMR and MALDI-TOF mass spectroscopy. |
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