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Efficient Microwave Assisted Syntheses of 2,5-Diketopiperazines in Aqueous Media (†)

Aqueous in situ one-pot N-Boc-deprotection-cyclization of Nα-Boc-dipeptidyl-tert-butyl and methyl esters under microwave irradiation afforded 2,5-diketopiperazines (DKPs) in excellent yields. This protocol is rapid, safe, environmentally friendly, and highly efficient, and showed that the tert-butox...

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Detalles Bibliográficos
Autores principales: Pérez-Picaso, Lemuel, Escalante, Jaime, Olivo, Horacio F., Rios, María Yolanda
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Molecular Diversity Preservation International 2009
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6254787/
https://www.ncbi.nlm.nih.gov/pubmed/19701127
http://dx.doi.org/10.3390/molecules14082836

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