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Analysis of the Chemical Composition of the Essential Oil of Polygonum minus Huds. Using Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry (GC-TOF MS)

The essential oil in leaves of Polygonum minus Huds., a local aromatic plant, were identified by a pipeline of gas chromatography (GC) techniques coupled with mass-spectrometry (MS), flame ionization detector (FID) and two dimensional gas chromatography time of flight mass spectrometry (GC×GC–TOF MS...

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Autores principales: Baharum, Syarul Nataqain, Bunawan, Hamidun, Ghani, Ma’aruf Abd., Mustapha, Wan Aida Wan, Noor, Normah Mohd
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2010
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6259174/
https://www.ncbi.nlm.nih.gov/pubmed/20944520
http://dx.doi.org/10.3390/molecules15107006
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author Baharum, Syarul Nataqain
Bunawan, Hamidun
Ghani, Ma’aruf Abd.
Mustapha, Wan Aida Wan
Noor, Normah Mohd
author_facet Baharum, Syarul Nataqain
Bunawan, Hamidun
Ghani, Ma’aruf Abd.
Mustapha, Wan Aida Wan
Noor, Normah Mohd
author_sort Baharum, Syarul Nataqain
collection PubMed
description The essential oil in leaves of Polygonum minus Huds., a local aromatic plant, were identified by a pipeline of gas chromatography (GC) techniques coupled with mass-spectrometry (MS), flame ionization detector (FID) and two dimensional gas chromatography time of flight mass spectrometry (GC×GC–TOF MS). A total of 48 compounds with a good match and high probability values were identified using this technique. Meanwhile, 42 compounds were successfully identified in this study using GC-MS, a significantly larger number than in previous studies. GC-FID was used in determining the retention indices of chemical components in P. minus essential oil. The result also showed the efficiency and reliability were greatly improved when chemometric methods and retention indices were used in identification and quantification of chemical components in plant essential oil.
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spelling pubmed-62591742018-12-06 Analysis of the Chemical Composition of the Essential Oil of Polygonum minus Huds. Using Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry (GC-TOF MS) Baharum, Syarul Nataqain Bunawan, Hamidun Ghani, Ma’aruf Abd. Mustapha, Wan Aida Wan Noor, Normah Mohd Molecules Article The essential oil in leaves of Polygonum minus Huds., a local aromatic plant, were identified by a pipeline of gas chromatography (GC) techniques coupled with mass-spectrometry (MS), flame ionization detector (FID) and two dimensional gas chromatography time of flight mass spectrometry (GC×GC–TOF MS). A total of 48 compounds with a good match and high probability values were identified using this technique. Meanwhile, 42 compounds were successfully identified in this study using GC-MS, a significantly larger number than in previous studies. GC-FID was used in determining the retention indices of chemical components in P. minus essential oil. The result also showed the efficiency and reliability were greatly improved when chemometric methods and retention indices were used in identification and quantification of chemical components in plant essential oil. MDPI 2010-10-12 /pmc/articles/PMC6259174/ /pubmed/20944520 http://dx.doi.org/10.3390/molecules15107006 Text en © 2010 by the authors; http://creativecommons.org/licenses/by/3.0/ licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution license (http://creativecommons.org/licenses/by/3.0/).
spellingShingle Article
Baharum, Syarul Nataqain
Bunawan, Hamidun
Ghani, Ma’aruf Abd.
Mustapha, Wan Aida Wan
Noor, Normah Mohd
Analysis of the Chemical Composition of the Essential Oil of Polygonum minus Huds. Using Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry (GC-TOF MS)
title Analysis of the Chemical Composition of the Essential Oil of Polygonum minus Huds. Using Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry (GC-TOF MS)
title_full Analysis of the Chemical Composition of the Essential Oil of Polygonum minus Huds. Using Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry (GC-TOF MS)
title_fullStr Analysis of the Chemical Composition of the Essential Oil of Polygonum minus Huds. Using Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry (GC-TOF MS)
title_full_unstemmed Analysis of the Chemical Composition of the Essential Oil of Polygonum minus Huds. Using Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry (GC-TOF MS)
title_short Analysis of the Chemical Composition of the Essential Oil of Polygonum minus Huds. Using Two-Dimensional Gas Chromatography-Time-of-Flight Mass Spectrometry (GC-TOF MS)
title_sort analysis of the chemical composition of the essential oil of polygonum minus huds. using two-dimensional gas chromatography-time-of-flight mass spectrometry (gc-tof ms)
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6259174/
https://www.ncbi.nlm.nih.gov/pubmed/20944520
http://dx.doi.org/10.3390/molecules15107006
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