Cargando…
Synthesis of New Azo Compounds Based on N-(4-Hydroxypheneyl)maleimide and N-(4-Methylpheneyl)maleimide
Maleic anhydride was reacted with p-aminophenol and p-toluidine in the presence of di-phosphorus pentoxide (P(2)O(5)) as a catalyst to produce two compounds: N-(4-hydroxy-phenyl)maleimide (I) and N-(4-methylphenyl)maleimide (II). The new azo compounds I(a-c) and II(a-c) were prepared by the reaction...
Autores principales: | , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2010
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6259232/ https://www.ncbi.nlm.nih.gov/pubmed/20975631 http://dx.doi.org/10.3390/molecules15107498 |
_version_ | 1783374639192342528 |
---|---|
author | Mohammed, Issam Ahmed Mustapha, Asniza |
author_facet | Mohammed, Issam Ahmed Mustapha, Asniza |
author_sort | Mohammed, Issam Ahmed |
collection | PubMed |
description | Maleic anhydride was reacted with p-aminophenol and p-toluidine in the presence of di-phosphorus pentoxide (P(2)O(5)) as a catalyst to produce two compounds: N-(4-hydroxy-phenyl)maleimide (I) and N-(4-methylphenyl)maleimide (II). The new azo compounds I(a-c) and II(a-c) were prepared by the reaction of I and II with three different aromatic amines, namely aniline, p-aminophenol and p-toluidine. The structures of these compounds were confirmed by CHN, FT-IR, (1)H-NMR, (13)C-NMR, mass spectrum and UV/Vis spectroscopy. |
format | Online Article Text |
id | pubmed-6259232 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2010 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-62592322018-12-06 Synthesis of New Azo Compounds Based on N-(4-Hydroxypheneyl)maleimide and N-(4-Methylpheneyl)maleimide Mohammed, Issam Ahmed Mustapha, Asniza Molecules Article Maleic anhydride was reacted with p-aminophenol and p-toluidine in the presence of di-phosphorus pentoxide (P(2)O(5)) as a catalyst to produce two compounds: N-(4-hydroxy-phenyl)maleimide (I) and N-(4-methylphenyl)maleimide (II). The new azo compounds I(a-c) and II(a-c) were prepared by the reaction of I and II with three different aromatic amines, namely aniline, p-aminophenol and p-toluidine. The structures of these compounds were confirmed by CHN, FT-IR, (1)H-NMR, (13)C-NMR, mass spectrum and UV/Vis spectroscopy. MDPI 2010-10-25 /pmc/articles/PMC6259232/ /pubmed/20975631 http://dx.doi.org/10.3390/molecules15107498 Text en © 2010 by the authors; http://creativecommons.org/licenses/by/3.0/ licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution license (http://creativecommons.org/licenses/by/3.0/). |
spellingShingle | Article Mohammed, Issam Ahmed Mustapha, Asniza Synthesis of New Azo Compounds Based on N-(4-Hydroxypheneyl)maleimide and N-(4-Methylpheneyl)maleimide |
title | Synthesis of New Azo Compounds Based on N-(4-Hydroxypheneyl)maleimide and N-(4-Methylpheneyl)maleimide |
title_full | Synthesis of New Azo Compounds Based on N-(4-Hydroxypheneyl)maleimide and N-(4-Methylpheneyl)maleimide |
title_fullStr | Synthesis of New Azo Compounds Based on N-(4-Hydroxypheneyl)maleimide and N-(4-Methylpheneyl)maleimide |
title_full_unstemmed | Synthesis of New Azo Compounds Based on N-(4-Hydroxypheneyl)maleimide and N-(4-Methylpheneyl)maleimide |
title_short | Synthesis of New Azo Compounds Based on N-(4-Hydroxypheneyl)maleimide and N-(4-Methylpheneyl)maleimide |
title_sort | synthesis of new azo compounds based on n-(4-hydroxypheneyl)maleimide and n-(4-methylpheneyl)maleimide |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6259232/ https://www.ncbi.nlm.nih.gov/pubmed/20975631 http://dx.doi.org/10.3390/molecules15107498 |
work_keys_str_mv | AT mohammedissamahmed synthesisofnewazocompoundsbasedonn4hydroxypheneylmaleimideandn4methylpheneylmaleimide AT mustaphaasniza synthesisofnewazocompoundsbasedonn4hydroxypheneylmaleimideandn4methylpheneylmaleimide |