Fast Method for Synthesis of Alkyl and Aryl-N-Methylnitrones

A simple, fast, efficient and eco-friendly procedure was developed for the synthesis of alkyl and aryl-N-methylnitrones. The corresponding nitrones of aromatic aldehydes, aliphatic aldehydes and alicyclic carbonyl compounds were prepared from N-methylhydroxylamine hydrochloride and Na(2)CO(3)-Na(2)S...

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Detalles Bibliográficos
Autores principales: Yavuz, Serkan, Ozkan, Hamdi, Colak, Naki, Yildirir, Yilmaz
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2011
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6264226/
https://www.ncbi.nlm.nih.gov/pubmed/25134771
http://dx.doi.org/10.3390/molecules16086677
Descripción
Sumario:A simple, fast, efficient and eco-friendly procedure was developed for the synthesis of alkyl and aryl-N-methylnitrones. The corresponding nitrones of aromatic aldehydes, aliphatic aldehydes and alicyclic carbonyl compounds were prepared from N-methylhydroxylamine hydrochloride and Na(2)CO(3)-Na(2)SO(4) by simply grinding at room temperature without using solvent.

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