Fast Method for Synthesis of Alkyl and Aryl-N-Methylnitrones

A simple, fast, efficient and eco-friendly procedure was developed for the synthesis of alkyl and aryl-N-methylnitrones. The corresponding nitrones of aromatic aldehydes, aliphatic aldehydes and alicyclic carbonyl compounds were prepared from N-methylhydroxylamine hydrochloride and Na(2)CO(3)-Na(2)S...

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Detalles Bibliográficos
Autores principales: Yavuz, Serkan, Ozkan, Hamdi, Colak, Naki, Yildirir, Yilmaz
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2011
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6264226/
https://www.ncbi.nlm.nih.gov/pubmed/25134771
http://dx.doi.org/10.3390/molecules16086677
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author Yavuz, Serkan
Ozkan, Hamdi
Colak, Naki
Yildirir, Yilmaz
author_facet Yavuz, Serkan
Ozkan, Hamdi
Colak, Naki
Yildirir, Yilmaz
author_sort Yavuz, Serkan
collection PubMed
description A simple, fast, efficient and eco-friendly procedure was developed for the synthesis of alkyl and aryl-N-methylnitrones. The corresponding nitrones of aromatic aldehydes, aliphatic aldehydes and alicyclic carbonyl compounds were prepared from N-methylhydroxylamine hydrochloride and Na(2)CO(3)-Na(2)SO(4) by simply grinding at room temperature without using solvent.
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spelling pubmed-62642262018-12-10 Fast Method for Synthesis of Alkyl and Aryl-N-Methylnitrones Yavuz, Serkan Ozkan, Hamdi Colak, Naki Yildirir, Yilmaz Molecules Article A simple, fast, efficient and eco-friendly procedure was developed for the synthesis of alkyl and aryl-N-methylnitrones. The corresponding nitrones of aromatic aldehydes, aliphatic aldehydes and alicyclic carbonyl compounds were prepared from N-methylhydroxylamine hydrochloride and Na(2)CO(3)-Na(2)SO(4) by simply grinding at room temperature without using solvent. MDPI 2011-08-08 /pmc/articles/PMC6264226/ /pubmed/25134771 http://dx.doi.org/10.3390/molecules16086677 Text en © 2011 by the authors; licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution license (http://creativecommons.org/licenses/by/3.0/).
spellingShingle Article
Yavuz, Serkan
Ozkan, Hamdi
Colak, Naki
Yildirir, Yilmaz
Fast Method for Synthesis of Alkyl and Aryl-N-Methylnitrones
title Fast Method for Synthesis of Alkyl and Aryl-N-Methylnitrones
title_full Fast Method for Synthesis of Alkyl and Aryl-N-Methylnitrones
title_fullStr Fast Method for Synthesis of Alkyl and Aryl-N-Methylnitrones
title_full_unstemmed Fast Method for Synthesis of Alkyl and Aryl-N-Methylnitrones
title_short Fast Method for Synthesis of Alkyl and Aryl-N-Methylnitrones
title_sort fast method for synthesis of alkyl and aryl-n-methylnitrones
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6264226/
https://www.ncbi.nlm.nih.gov/pubmed/25134771
http://dx.doi.org/10.3390/molecules16086677
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AT ozkanhamdi fastmethodforsynthesisofalkylandarylnmethylnitrones
AT colaknaki fastmethodforsynthesisofalkylandarylnmethylnitrones
AT yildiriryilmaz fastmethodforsynthesisofalkylandarylnmethylnitrones

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