Determining Optimum Conditions for Lipase-Catalyzed Synthesis of Triethanolamine (TEA)-Based Esterquat Cationic Surfactant by a Taguchi Robust Design Method

A Taguchi robust design method with an L(9) orthogonal array was implemented to optimize experimental conditions for the biosynthesis of triethanolamine (TEA)-based esterquat cationic surfactants using an enzymatic reaction method. The esterification reaction conversion% was considered as the respon...

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Autores principales: Masoumi, Hamid Reza Fard, Kassim, Anuar, Basri, Mahiran, Abdullah, Dzulkifly Kuang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2011
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6264298/
https://www.ncbi.nlm.nih.gov/pubmed/21642941
http://dx.doi.org/10.3390/molecules16064672
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author Masoumi, Hamid Reza Fard
Kassim, Anuar
Basri, Mahiran
Abdullah, Dzulkifly Kuang
author_facet Masoumi, Hamid Reza Fard
Kassim, Anuar
Basri, Mahiran
Abdullah, Dzulkifly Kuang
author_sort Masoumi, Hamid Reza Fard
collection PubMed
description A Taguchi robust design method with an L(9) orthogonal array was implemented to optimize experimental conditions for the biosynthesis of triethanolamine (TEA)-based esterquat cationic surfactants using an enzymatic reaction method. The esterification reaction conversion% was considered as the response. Enzyme amount, reaction time, reaction temperature and molar ratio of substrates, [oleic acid: triethanolamine (OA:TEA)] were chosen as main parameters. As a result of the Taguchi analysis in this study, the molar ratio of substrates was found to be the most influential parameter on the esterification reaction conversion%. The amount of enzyme in the reaction had also a significant effect on reaction conversion%.
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spelling pubmed-62642982018-12-10 Determining Optimum Conditions for Lipase-Catalyzed Synthesis of Triethanolamine (TEA)-Based Esterquat Cationic Surfactant by a Taguchi Robust Design Method Masoumi, Hamid Reza Fard Kassim, Anuar Basri, Mahiran Abdullah, Dzulkifly Kuang Molecules Article A Taguchi robust design method with an L(9) orthogonal array was implemented to optimize experimental conditions for the biosynthesis of triethanolamine (TEA)-based esterquat cationic surfactants using an enzymatic reaction method. The esterification reaction conversion% was considered as the response. Enzyme amount, reaction time, reaction temperature and molar ratio of substrates, [oleic acid: triethanolamine (OA:TEA)] were chosen as main parameters. As a result of the Taguchi analysis in this study, the molar ratio of substrates was found to be the most influential parameter on the esterification reaction conversion%. The amount of enzyme in the reaction had also a significant effect on reaction conversion%. MDPI 2011-06-03 /pmc/articles/PMC6264298/ /pubmed/21642941 http://dx.doi.org/10.3390/molecules16064672 Text en © 2011 by the authors; licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution license (http://creativecommons.org/licenses/by/3.0/).
spellingShingle Article
Masoumi, Hamid Reza Fard
Kassim, Anuar
Basri, Mahiran
Abdullah, Dzulkifly Kuang
Determining Optimum Conditions for Lipase-Catalyzed Synthesis of Triethanolamine (TEA)-Based Esterquat Cationic Surfactant by a Taguchi Robust Design Method
title Determining Optimum Conditions for Lipase-Catalyzed Synthesis of Triethanolamine (TEA)-Based Esterquat Cationic Surfactant by a Taguchi Robust Design Method
title_full Determining Optimum Conditions for Lipase-Catalyzed Synthesis of Triethanolamine (TEA)-Based Esterquat Cationic Surfactant by a Taguchi Robust Design Method
title_fullStr Determining Optimum Conditions for Lipase-Catalyzed Synthesis of Triethanolamine (TEA)-Based Esterquat Cationic Surfactant by a Taguchi Robust Design Method
title_full_unstemmed Determining Optimum Conditions for Lipase-Catalyzed Synthesis of Triethanolamine (TEA)-Based Esterquat Cationic Surfactant by a Taguchi Robust Design Method
title_short Determining Optimum Conditions for Lipase-Catalyzed Synthesis of Triethanolamine (TEA)-Based Esterquat Cationic Surfactant by a Taguchi Robust Design Method
title_sort determining optimum conditions for lipase-catalyzed synthesis of triethanolamine (tea)-based esterquat cationic surfactant by a taguchi robust design method
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6264298/
https://www.ncbi.nlm.nih.gov/pubmed/21642941
http://dx.doi.org/10.3390/molecules16064672
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