Cargando…

A Facile Synthesis of Arylazonicotinates for Dyeing Polyester Fabrics under Microwave Irradiation and Their Biological Activity Profiles

A as textile dyes and the fastness properties of the dyed samples were measured. Most of the dyed fabrics tested displayed very good washing and perspiration fastness and series of 2-hydroxy- and 2-amino-6-substituted-5-arylazonicotinate monoazo compounds 7a–e and 9a–c were prepared via condensation...

Descripción completa

Detalles Bibliográficos
Autores principales: Al-Mousawi, Saleh M., El-Apasery, Morsy A., Mahmoud, Huda M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2012
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6268463/
https://www.ncbi.nlm.nih.gov/pubmed/23018924
http://dx.doi.org/10.3390/molecules171011495
_version_ 1783376292832346112
author Al-Mousawi, Saleh M.
El-Apasery, Morsy A.
Mahmoud, Huda M.
author_facet Al-Mousawi, Saleh M.
El-Apasery, Morsy A.
Mahmoud, Huda M.
author_sort Al-Mousawi, Saleh M.
collection PubMed
description A as textile dyes and the fastness properties of the dyed samples were measured. Most of the dyed fabrics tested displayed very good washing and perspiration fastness and series of 2-hydroxy- and 2-amino-6-substituted-5-arylazonicotinate monoazo compounds 7a–e and 9a–c were prepared via condensation of 3-oxo-3-substituted-2-arylhydrazonals 2a–e with active methylene nitriles 3a–d using microwave irradiation as an energy source. These substances were then tested moderate light fastness. Finally, the biological activity of the synthesized compounds against Gram positive bacteria, Gram negative bacteria and yeast were evaluated.
format Online
Article
Text
id pubmed-6268463
institution National Center for Biotechnology Information
language English
publishDate 2012
publisher MDPI
record_format MEDLINE/PubMed
spelling pubmed-62684632018-12-12 A Facile Synthesis of Arylazonicotinates for Dyeing Polyester Fabrics under Microwave Irradiation and Their Biological Activity Profiles Al-Mousawi, Saleh M. El-Apasery, Morsy A. Mahmoud, Huda M. Molecules Article A as textile dyes and the fastness properties of the dyed samples were measured. Most of the dyed fabrics tested displayed very good washing and perspiration fastness and series of 2-hydroxy- and 2-amino-6-substituted-5-arylazonicotinate monoazo compounds 7a–e and 9a–c were prepared via condensation of 3-oxo-3-substituted-2-arylhydrazonals 2a–e with active methylene nitriles 3a–d using microwave irradiation as an energy source. These substances were then tested moderate light fastness. Finally, the biological activity of the synthesized compounds against Gram positive bacteria, Gram negative bacteria and yeast were evaluated. MDPI 2012-09-27 /pmc/articles/PMC6268463/ /pubmed/23018924 http://dx.doi.org/10.3390/molecules171011495 Text en © 2012 by the authors; licensee MDPI, Basel, Switzerland. http://creativecommons.org/licenses/by/3.0/ This article is an open-access article distributed under the terms and conditions of the Creative Commons Attribution license (http://creativecommons.org/licenses/by/3.0/).
spellingShingle Article
Al-Mousawi, Saleh M.
El-Apasery, Morsy A.
Mahmoud, Huda M.
A Facile Synthesis of Arylazonicotinates for Dyeing Polyester Fabrics under Microwave Irradiation and Their Biological Activity Profiles
title A Facile Synthesis of Arylazonicotinates for Dyeing Polyester Fabrics under Microwave Irradiation and Their Biological Activity Profiles
title_full A Facile Synthesis of Arylazonicotinates for Dyeing Polyester Fabrics under Microwave Irradiation and Their Biological Activity Profiles
title_fullStr A Facile Synthesis of Arylazonicotinates for Dyeing Polyester Fabrics under Microwave Irradiation and Their Biological Activity Profiles
title_full_unstemmed A Facile Synthesis of Arylazonicotinates for Dyeing Polyester Fabrics under Microwave Irradiation and Their Biological Activity Profiles
title_short A Facile Synthesis of Arylazonicotinates for Dyeing Polyester Fabrics under Microwave Irradiation and Their Biological Activity Profiles
title_sort facile synthesis of arylazonicotinates for dyeing polyester fabrics under microwave irradiation and their biological activity profiles
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6268463/
https://www.ncbi.nlm.nih.gov/pubmed/23018924
http://dx.doi.org/10.3390/molecules171011495
work_keys_str_mv AT almousawisalehm afacilesynthesisofarylazonicotinatesfordyeingpolyesterfabricsundermicrowaveirradiationandtheirbiologicalactivityprofiles
AT elapaserymorsya afacilesynthesisofarylazonicotinatesfordyeingpolyesterfabricsundermicrowaveirradiationandtheirbiologicalactivityprofiles
AT mahmoudhudam afacilesynthesisofarylazonicotinatesfordyeingpolyesterfabricsundermicrowaveirradiationandtheirbiologicalactivityprofiles
AT almousawisalehm facilesynthesisofarylazonicotinatesfordyeingpolyesterfabricsundermicrowaveirradiationandtheirbiologicalactivityprofiles
AT elapaserymorsya facilesynthesisofarylazonicotinatesfordyeingpolyesterfabricsundermicrowaveirradiationandtheirbiologicalactivityprofiles
AT mahmoudhudam facilesynthesisofarylazonicotinatesfordyeingpolyesterfabricsundermicrowaveirradiationandtheirbiologicalactivityprofiles