Synthesis and NMR Spectral Studies of the 7-C(60)-Adduct of N,N-(Tetrachlorophthaloyl) Dehydroabietylamine

The 7-C(60)-adduct of N,N-(tetrachlorophthaloyl)dehydroabietylamine was synthesized for the first time and characterized by IR, UV-vis, mass and NMR spectral studies. The (1)H-NMR and (13)C-NMR resonance signals of the new compound are unambiguously assigned by using homo- and heteronuclear 2D NMR s...

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Detalles Bibliográficos
Autores principales: Zhou, Zhi, Lin, Zhongxiang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2012
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6268738/
https://www.ncbi.nlm.nih.gov/pubmed/22481541
http://dx.doi.org/10.3390/molecules17044209
Descripción
Sumario:The 7-C(60)-adduct of N,N-(tetrachlorophthaloyl)dehydroabietylamine was synthesized for the first time and characterized by IR, UV-vis, mass and NMR spectral studies. The (1)H-NMR and (13)C-NMR resonance signals of the new compound are unambiguously assigned by using homo- and heteronuclear 2D NMR spectroscopic techniques such as COSY, ROESY, HSQC and HMBC. The C(1) symmetric structure with 6,6-junction of compound was determined.

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