Cargando…
Synthesis and NMR Spectral Studies of the 7-C(60)-Adduct of N,N-(Tetrachlorophthaloyl) Dehydroabietylamine
The 7-C(60)-adduct of N,N-(tetrachlorophthaloyl)dehydroabietylamine was synthesized for the first time and characterized by IR, UV-vis, mass and NMR spectral studies. The (1)H-NMR and (13)C-NMR resonance signals of the new compound are unambiguously assigned by using homo- and heteronuclear 2D NMR s...
Autores principales: | , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2012
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6268738/ https://www.ncbi.nlm.nih.gov/pubmed/22481541 http://dx.doi.org/10.3390/molecules17044209 |
_version_ | 1783376355463790592 |
---|---|
author | Zhou, Zhi Lin, Zhongxiang |
author_facet | Zhou, Zhi Lin, Zhongxiang |
author_sort | Zhou, Zhi |
collection | PubMed |
description | The 7-C(60)-adduct of N,N-(tetrachlorophthaloyl)dehydroabietylamine was synthesized for the first time and characterized by IR, UV-vis, mass and NMR spectral studies. The (1)H-NMR and (13)C-NMR resonance signals of the new compound are unambiguously assigned by using homo- and heteronuclear 2D NMR spectroscopic techniques such as COSY, ROESY, HSQC and HMBC. The C(1) symmetric structure with 6,6-junction of compound was determined. |
format | Online Article Text |
id | pubmed-6268738 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2012 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-62687382018-12-11 Synthesis and NMR Spectral Studies of the 7-C(60)-Adduct of N,N-(Tetrachlorophthaloyl) Dehydroabietylamine Zhou, Zhi Lin, Zhongxiang Molecules Article The 7-C(60)-adduct of N,N-(tetrachlorophthaloyl)dehydroabietylamine was synthesized for the first time and characterized by IR, UV-vis, mass and NMR spectral studies. The (1)H-NMR and (13)C-NMR resonance signals of the new compound are unambiguously assigned by using homo- and heteronuclear 2D NMR spectroscopic techniques such as COSY, ROESY, HSQC and HMBC. The C(1) symmetric structure with 6,6-junction of compound was determined. MDPI 2012-04-05 /pmc/articles/PMC6268738/ /pubmed/22481541 http://dx.doi.org/10.3390/molecules17044209 Text en © 2012 by the authors; licensee MDPI, Basel, Switzerland. http://creativecommons.org/licenses/by/3.0/ This article is an open-access article distributed under the terms and conditions of the Creative Commons Attribution license (http://creativecommons.org/licenses/by/3.0/). |
spellingShingle | Article Zhou, Zhi Lin, Zhongxiang Synthesis and NMR Spectral Studies of the 7-C(60)-Adduct of N,N-(Tetrachlorophthaloyl) Dehydroabietylamine |
title | Synthesis and NMR Spectral Studies of the 7-C(60)-Adduct of N,N-(Tetrachlorophthaloyl) Dehydroabietylamine |
title_full | Synthesis and NMR Spectral Studies of the 7-C(60)-Adduct of N,N-(Tetrachlorophthaloyl) Dehydroabietylamine |
title_fullStr | Synthesis and NMR Spectral Studies of the 7-C(60)-Adduct of N,N-(Tetrachlorophthaloyl) Dehydroabietylamine |
title_full_unstemmed | Synthesis and NMR Spectral Studies of the 7-C(60)-Adduct of N,N-(Tetrachlorophthaloyl) Dehydroabietylamine |
title_short | Synthesis and NMR Spectral Studies of the 7-C(60)-Adduct of N,N-(Tetrachlorophthaloyl) Dehydroabietylamine |
title_sort | synthesis and nmr spectral studies of the 7-c(60)-adduct of n,n-(tetrachlorophthaloyl) dehydroabietylamine |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6268738/ https://www.ncbi.nlm.nih.gov/pubmed/22481541 http://dx.doi.org/10.3390/molecules17044209 |
work_keys_str_mv | AT zhouzhi synthesisandnmrspectralstudiesofthe7c60adductofnntetrachlorophthaloyldehydroabietylamine AT linzhongxiang synthesisandnmrspectralstudiesofthe7c60adductofnntetrachlorophthaloyldehydroabietylamine |