Graphite-Supported Perchloric Acid (HClO(4)-C): An Efficient and Recyclable Heterogeneous Catalyst for the One-Pot Synthesis of Amidoalkyl Naphthols

An efficient and direct protocol for the preparation of amidoalkylnaphthols employing a multi-component, one-pot condensation reaction of 2-naphthol, aromatic aldehydes and acetamide or benzamide in the presence of graphite supported perchloric acid under solvent-free conditions is described. The th...

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Detalles Bibliográficos
Autores principales: Lei, Zhen-Kai, Xiao, Li, Lu, Xiao-Quan, Huang, He, Liu, Chen-Jiang
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2013
Materias:
Article
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6270571/
https://www.ncbi.nlm.nih.gov/pubmed/23358323
http://dx.doi.org/10.3390/molecules18021653
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author Lei, Zhen-Kai
Xiao, Li
Lu, Xiao-Quan
Huang, He
Liu, Chen-Jiang
author_facet Lei, Zhen-Kai
Xiao, Li
Lu, Xiao-Quan
Huang, He
Liu, Chen-Jiang
author_sort Lei, Zhen-Kai
collection PubMed
description An efficient and direct protocol for the preparation of amidoalkylnaphthols employing a multi-component, one-pot condensation reaction of 2-naphthol, aromatic aldehydes and acetamide or benzamide in the presence of graphite supported perchloric acid under solvent-free conditions is described. The thermal solvent-free procedure offers advantages such as simple work-up, shorter reaction times and higher product yields, and the catalyst exhibited remarkable reactivity and can be recycled.
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spelling pubmed-62705712018-12-14 Graphite-Supported Perchloric Acid (HClO(4)-C): An Efficient and Recyclable Heterogeneous Catalyst for the One-Pot Synthesis of Amidoalkyl Naphthols Lei, Zhen-Kai Xiao, Li Lu, Xiao-Quan Huang, He Liu, Chen-Jiang Molecules Article An efficient and direct protocol for the preparation of amidoalkylnaphthols employing a multi-component, one-pot condensation reaction of 2-naphthol, aromatic aldehydes and acetamide or benzamide in the presence of graphite supported perchloric acid under solvent-free conditions is described. The thermal solvent-free procedure offers advantages such as simple work-up, shorter reaction times and higher product yields, and the catalyst exhibited remarkable reactivity and can be recycled. MDPI 2013-01-28 /pmc/articles/PMC6270571/ /pubmed/23358323 http://dx.doi.org/10.3390/molecules18021653 Text en © 2013 by the authors; licensee MDPI, Basel, Switzerland. http://creativecommons.org/licenses/by/3.0/ This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution license (http://creativecommons.org/licenses/by/3.0/).
spellingShingle Article
Lei, Zhen-Kai
Xiao, Li
Lu, Xiao-Quan
Huang, He
Liu, Chen-Jiang
Graphite-Supported Perchloric Acid (HClO(4)-C): An Efficient and Recyclable Heterogeneous Catalyst for the One-Pot Synthesis of Amidoalkyl Naphthols
title Graphite-Supported Perchloric Acid (HClO(4)-C): An Efficient and Recyclable Heterogeneous Catalyst for the One-Pot Synthesis of Amidoalkyl Naphthols
title_full Graphite-Supported Perchloric Acid (HClO(4)-C): An Efficient and Recyclable Heterogeneous Catalyst for the One-Pot Synthesis of Amidoalkyl Naphthols
title_fullStr Graphite-Supported Perchloric Acid (HClO(4)-C): An Efficient and Recyclable Heterogeneous Catalyst for the One-Pot Synthesis of Amidoalkyl Naphthols
title_full_unstemmed Graphite-Supported Perchloric Acid (HClO(4)-C): An Efficient and Recyclable Heterogeneous Catalyst for the One-Pot Synthesis of Amidoalkyl Naphthols
title_short Graphite-Supported Perchloric Acid (HClO(4)-C): An Efficient and Recyclable Heterogeneous Catalyst for the One-Pot Synthesis of Amidoalkyl Naphthols
title_sort graphite-supported perchloric acid (hclo(4)-c): an efficient and recyclable heterogeneous catalyst for the one-pot synthesis of amidoalkyl naphthols
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6270571/
https://www.ncbi.nlm.nih.gov/pubmed/23358323
http://dx.doi.org/10.3390/molecules18021653
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