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Synthesis of Stabilized Myrrh-Capped Hydrocolloidal Magnetite Nanoparticles

Herein we report a new method for synthesizing stabilized magnetic nanoparticle (MNP) colloids. A new class of monodisperse water-soluble magnetite nano-particles was prepared by a simple and inexpensive co-precipitation method. Iron ions and iodine were prepared by the reaction between ferric chlor...

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Autores principales: Atta, Ayman M., Al-Lohedan, Hamad A., Al-Hussain, Sami A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2014
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6271377/
https://www.ncbi.nlm.nih.gov/pubmed/25090117
http://dx.doi.org/10.3390/molecules190811263
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author Atta, Ayman M.
Al-Lohedan, Hamad A.
Al-Hussain, Sami A.
author_facet Atta, Ayman M.
Al-Lohedan, Hamad A.
Al-Hussain, Sami A.
author_sort Atta, Ayman M.
collection PubMed
description Herein we report a new method for synthesizing stabilized magnetic nanoparticle (MNP) colloids. A new class of monodisperse water-soluble magnetite nano-particles was prepared by a simple and inexpensive co-precipitation method. Iron ions and iodine were prepared by the reaction between ferric chloride and potassium iodide. The ferrous and ferric ions were hydrolyzed at low temperature at pH 9 in the presence of iodine to produce iron oxide nanoparticles. The natural product myrrh gum was used as capping agent to produce highly dispersed coated magnetite nanoparticles. The structure and morphology of the magnetic nanogel was characterized by Fourier transform infrared spectroscopy (FTIR) and transmission electron microscopy (TEM), and X-ray diffraction (XRD) was used to examine the crystal structure of the produced magnetite nanoparticles.
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spelling pubmed-62713772018-12-27 Synthesis of Stabilized Myrrh-Capped Hydrocolloidal Magnetite Nanoparticles Atta, Ayman M. Al-Lohedan, Hamad A. Al-Hussain, Sami A. Molecules Article Herein we report a new method for synthesizing stabilized magnetic nanoparticle (MNP) colloids. A new class of monodisperse water-soluble magnetite nano-particles was prepared by a simple and inexpensive co-precipitation method. Iron ions and iodine were prepared by the reaction between ferric chloride and potassium iodide. The ferrous and ferric ions were hydrolyzed at low temperature at pH 9 in the presence of iodine to produce iron oxide nanoparticles. The natural product myrrh gum was used as capping agent to produce highly dispersed coated magnetite nanoparticles. The structure and morphology of the magnetic nanogel was characterized by Fourier transform infrared spectroscopy (FTIR) and transmission electron microscopy (TEM), and X-ray diffraction (XRD) was used to examine the crystal structure of the produced magnetite nanoparticles. MDPI 2014-07-31 /pmc/articles/PMC6271377/ /pubmed/25090117 http://dx.doi.org/10.3390/molecules190811263 Text en © 2014 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution license (http://creativecommons.org/licenses/by/3.0/).
spellingShingle Article
Atta, Ayman M.
Al-Lohedan, Hamad A.
Al-Hussain, Sami A.
Synthesis of Stabilized Myrrh-Capped Hydrocolloidal Magnetite Nanoparticles
title Synthesis of Stabilized Myrrh-Capped Hydrocolloidal Magnetite Nanoparticles
title_full Synthesis of Stabilized Myrrh-Capped Hydrocolloidal Magnetite Nanoparticles
title_fullStr Synthesis of Stabilized Myrrh-Capped Hydrocolloidal Magnetite Nanoparticles
title_full_unstemmed Synthesis of Stabilized Myrrh-Capped Hydrocolloidal Magnetite Nanoparticles
title_short Synthesis of Stabilized Myrrh-Capped Hydrocolloidal Magnetite Nanoparticles
title_sort synthesis of stabilized myrrh-capped hydrocolloidal magnetite nanoparticles
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6271377/
https://www.ncbi.nlm.nih.gov/pubmed/25090117
http://dx.doi.org/10.3390/molecules190811263
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