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In Situ Investigation of a Self-Accelerated Cocrystal Formation by Grinding Pyrazinamide with Oxalic Acid
A new cocrystal of pyrazinamide with oxalic acid was prepared mechanochemically and characterized by PXRD, Raman spectroscopy, solid-state NMR spectroscopy, DTA-TG, and SEM. Based on powder X-ray diffraction data the structure was solved. The formation pathway of the reaction was studied in situ usi...
Autores principales: | Kulla, Hannes, Greiser, Sebastian, Benemann, Sigrid, Rademann, Klaus, Emmerling, Franziska |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2016
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6274108/ https://www.ncbi.nlm.nih.gov/pubmed/27428942 http://dx.doi.org/10.3390/molecules21070917 |
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