Cargando…

Mechanical Properties and Microstructure of DMLS Ti6Al4V Alloy Dedicated to Biomedical Applications

The aim of this work was to investigate the microstructure and mechanical properties of samples produced by direct metal laser sintering (DMLS) with varied laser beam speed before and after heat treatment. Optical analysis of as-built samples revealed microstructure built of martensite needles and c...

Descripción completa

Detalles Bibliográficos
Autores principales: Mierzejewska, Żaneta Anna, Hudák, Radovan, Sidun, Jarosław
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6337110/
https://www.ncbi.nlm.nih.gov/pubmed/30621079
http://dx.doi.org/10.3390/ma12010176
_version_ 1783388168318353408
author Mierzejewska, Żaneta Anna
Hudák, Radovan
Sidun, Jarosław
author_facet Mierzejewska, Żaneta Anna
Hudák, Radovan
Sidun, Jarosław
author_sort Mierzejewska, Żaneta Anna
collection PubMed
description The aim of this work was to investigate the microstructure and mechanical properties of samples produced by direct metal laser sintering (DMLS) with varied laser beam speed before and after heat treatment. Optical analysis of as-built samples revealed microstructure built of martensite needles and columnar grains, growing epitaxially towards the built direction. External and internal pores, un-melted or semi-melted powder particles and inclusions in the examined samples were also observed. The strength and Young’s modulus of the DMLS samples before heat treatment was higher than for cast and forged samples; however, the elongation at break for vertical and horizontal orientation was lower than required for biomedical implants. After heat treatment, the hardness of the samples decreased, which is associated with the disappearance of boundary effect and martensite decomposition to lamellar mixture of α and β, and the anisotropic behaviour of the material also disappears. Ultimate tensile strength (UTS) and yield strength(YS) also decreased, while elongation increased. Tensile properties were sensitive to the build orientation, which indicates that DMLS generates anisotropy of material as a result of layered production and elongated β prior grains. It was noticed that inappropriate selection of parameters did not allow properties corresponding to the standards to be obtained due to the high porosity and defects of the microstructure caused by insufficient energy density.
format Online
Article
Text
id pubmed-6337110
institution National Center for Biotechnology Information
language English
publishDate 2019
publisher MDPI
record_format MEDLINE/PubMed
spelling pubmed-63371102019-01-22 Mechanical Properties and Microstructure of DMLS Ti6Al4V Alloy Dedicated to Biomedical Applications Mierzejewska, Żaneta Anna Hudák, Radovan Sidun, Jarosław Materials (Basel) Article The aim of this work was to investigate the microstructure and mechanical properties of samples produced by direct metal laser sintering (DMLS) with varied laser beam speed before and after heat treatment. Optical analysis of as-built samples revealed microstructure built of martensite needles and columnar grains, growing epitaxially towards the built direction. External and internal pores, un-melted or semi-melted powder particles and inclusions in the examined samples were also observed. The strength and Young’s modulus of the DMLS samples before heat treatment was higher than for cast and forged samples; however, the elongation at break for vertical and horizontal orientation was lower than required for biomedical implants. After heat treatment, the hardness of the samples decreased, which is associated with the disappearance of boundary effect and martensite decomposition to lamellar mixture of α and β, and the anisotropic behaviour of the material also disappears. Ultimate tensile strength (UTS) and yield strength(YS) also decreased, while elongation increased. Tensile properties were sensitive to the build orientation, which indicates that DMLS generates anisotropy of material as a result of layered production and elongated β prior grains. It was noticed that inappropriate selection of parameters did not allow properties corresponding to the standards to be obtained due to the high porosity and defects of the microstructure caused by insufficient energy density. MDPI 2019-01-07 /pmc/articles/PMC6337110/ /pubmed/30621079 http://dx.doi.org/10.3390/ma12010176 Text en © 2019 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Mierzejewska, Żaneta Anna
Hudák, Radovan
Sidun, Jarosław
Mechanical Properties and Microstructure of DMLS Ti6Al4V Alloy Dedicated to Biomedical Applications
title Mechanical Properties and Microstructure of DMLS Ti6Al4V Alloy Dedicated to Biomedical Applications
title_full Mechanical Properties and Microstructure of DMLS Ti6Al4V Alloy Dedicated to Biomedical Applications
title_fullStr Mechanical Properties and Microstructure of DMLS Ti6Al4V Alloy Dedicated to Biomedical Applications
title_full_unstemmed Mechanical Properties and Microstructure of DMLS Ti6Al4V Alloy Dedicated to Biomedical Applications
title_short Mechanical Properties and Microstructure of DMLS Ti6Al4V Alloy Dedicated to Biomedical Applications
title_sort mechanical properties and microstructure of dmls ti6al4v alloy dedicated to biomedical applications
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6337110/
https://www.ncbi.nlm.nih.gov/pubmed/30621079
http://dx.doi.org/10.3390/ma12010176
work_keys_str_mv AT mierzejewskazanetaanna mechanicalpropertiesandmicrostructureofdmlsti6al4valloydedicatedtobiomedicalapplications
AT hudakradovan mechanicalpropertiesandmicrostructureofdmlsti6al4valloydedicatedtobiomedicalapplications
AT sidunjarosław mechanicalpropertiesandmicrostructureofdmlsti6al4valloydedicatedtobiomedicalapplications