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Mechanical Properties and Microstructure of DMLS Ti6Al4V Alloy Dedicated to Biomedical Applications
The aim of this work was to investigate the microstructure and mechanical properties of samples produced by direct metal laser sintering (DMLS) with varied laser beam speed before and after heat treatment. Optical analysis of as-built samples revealed microstructure built of martensite needles and c...
Autores principales: | , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2019
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6337110/ https://www.ncbi.nlm.nih.gov/pubmed/30621079 http://dx.doi.org/10.3390/ma12010176 |
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author | Mierzejewska, Żaneta Anna Hudák, Radovan Sidun, Jarosław |
author_facet | Mierzejewska, Żaneta Anna Hudák, Radovan Sidun, Jarosław |
author_sort | Mierzejewska, Żaneta Anna |
collection | PubMed |
description | The aim of this work was to investigate the microstructure and mechanical properties of samples produced by direct metal laser sintering (DMLS) with varied laser beam speed before and after heat treatment. Optical analysis of as-built samples revealed microstructure built of martensite needles and columnar grains, growing epitaxially towards the built direction. External and internal pores, un-melted or semi-melted powder particles and inclusions in the examined samples were also observed. The strength and Young’s modulus of the DMLS samples before heat treatment was higher than for cast and forged samples; however, the elongation at break for vertical and horizontal orientation was lower than required for biomedical implants. After heat treatment, the hardness of the samples decreased, which is associated with the disappearance of boundary effect and martensite decomposition to lamellar mixture of α and β, and the anisotropic behaviour of the material also disappears. Ultimate tensile strength (UTS) and yield strength(YS) also decreased, while elongation increased. Tensile properties were sensitive to the build orientation, which indicates that DMLS generates anisotropy of material as a result of layered production and elongated β prior grains. It was noticed that inappropriate selection of parameters did not allow properties corresponding to the standards to be obtained due to the high porosity and defects of the microstructure caused by insufficient energy density. |
format | Online Article Text |
id | pubmed-6337110 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2019 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-63371102019-01-22 Mechanical Properties and Microstructure of DMLS Ti6Al4V Alloy Dedicated to Biomedical Applications Mierzejewska, Żaneta Anna Hudák, Radovan Sidun, Jarosław Materials (Basel) Article The aim of this work was to investigate the microstructure and mechanical properties of samples produced by direct metal laser sintering (DMLS) with varied laser beam speed before and after heat treatment. Optical analysis of as-built samples revealed microstructure built of martensite needles and columnar grains, growing epitaxially towards the built direction. External and internal pores, un-melted or semi-melted powder particles and inclusions in the examined samples were also observed. The strength and Young’s modulus of the DMLS samples before heat treatment was higher than for cast and forged samples; however, the elongation at break for vertical and horizontal orientation was lower than required for biomedical implants. After heat treatment, the hardness of the samples decreased, which is associated with the disappearance of boundary effect and martensite decomposition to lamellar mixture of α and β, and the anisotropic behaviour of the material also disappears. Ultimate tensile strength (UTS) and yield strength(YS) also decreased, while elongation increased. Tensile properties were sensitive to the build orientation, which indicates that DMLS generates anisotropy of material as a result of layered production and elongated β prior grains. It was noticed that inappropriate selection of parameters did not allow properties corresponding to the standards to be obtained due to the high porosity and defects of the microstructure caused by insufficient energy density. MDPI 2019-01-07 /pmc/articles/PMC6337110/ /pubmed/30621079 http://dx.doi.org/10.3390/ma12010176 Text en © 2019 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Mierzejewska, Żaneta Anna Hudák, Radovan Sidun, Jarosław Mechanical Properties and Microstructure of DMLS Ti6Al4V Alloy Dedicated to Biomedical Applications |
title | Mechanical Properties and Microstructure of DMLS Ti6Al4V Alloy Dedicated to Biomedical Applications |
title_full | Mechanical Properties and Microstructure of DMLS Ti6Al4V Alloy Dedicated to Biomedical Applications |
title_fullStr | Mechanical Properties and Microstructure of DMLS Ti6Al4V Alloy Dedicated to Biomedical Applications |
title_full_unstemmed | Mechanical Properties and Microstructure of DMLS Ti6Al4V Alloy Dedicated to Biomedical Applications |
title_short | Mechanical Properties and Microstructure of DMLS Ti6Al4V Alloy Dedicated to Biomedical Applications |
title_sort | mechanical properties and microstructure of dmls ti6al4v alloy dedicated to biomedical applications |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6337110/ https://www.ncbi.nlm.nih.gov/pubmed/30621079 http://dx.doi.org/10.3390/ma12010176 |
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