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Structural and Superconducting Properties of Thermal Treatment-Synthesised Bulk YBa(2)Cu(3)O(7−δ) Superconductor: Effect of Addition of SnO(2) Nanoparticles

YBa(2)Cu(3)O(7−δ) (Y-123) bulk superconductors with the addition of (0.0, 0.2, 0.4, 0.6, 0.8, and 1.0 wt.%) SnO(2) nanoparticles were synthesised via a thermal treatment method. The influence of SnO(2) addition on the superconducting properties by means of critical temperature, T(c), AC susceptibili...

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Autores principales: Mohd Yusuf, Nur Nabilah, Awang Kechik, Mohd Mustafa, Baqiah, Hussein, Soo Kien, Chen, Kean Pah, Lim, Shaari, Abdul Halim, Wan Jusoh, Wan Nur Wathiq, Abd Sukor, Safia Izzati, Mousa Dihom, Mustafa, Talib, Zainal Abidin, Abd-Shukor, Roslan
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2018
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6337648/
https://www.ncbi.nlm.nih.gov/pubmed/30597840
http://dx.doi.org/10.3390/ma12010092
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author Mohd Yusuf, Nur Nabilah
Awang Kechik, Mohd Mustafa
Baqiah, Hussein
Soo Kien, Chen
Kean Pah, Lim
Shaari, Abdul Halim
Wan Jusoh, Wan Nur Wathiq
Abd Sukor, Safia Izzati
Mousa Dihom, Mustafa
Talib, Zainal Abidin
Abd-Shukor, Roslan
author_facet Mohd Yusuf, Nur Nabilah
Awang Kechik, Mohd Mustafa
Baqiah, Hussein
Soo Kien, Chen
Kean Pah, Lim
Shaari, Abdul Halim
Wan Jusoh, Wan Nur Wathiq
Abd Sukor, Safia Izzati
Mousa Dihom, Mustafa
Talib, Zainal Abidin
Abd-Shukor, Roslan
author_sort Mohd Yusuf, Nur Nabilah
collection PubMed
description YBa(2)Cu(3)O(7−δ) (Y-123) bulk superconductors with the addition of (0.0, 0.2, 0.4, 0.6, 0.8, and 1.0 wt.%) SnO(2) nanoparticles were synthesised via a thermal treatment method. The influence of SnO(2) addition on the superconducting properties by means of critical temperature, T(c), AC susceptibility, phase formation and microstructures, including its elemental composition analysis, were studied. Sharp superconducting transition, ∆T(c), and diamagnetic transition were obtained for all SnO(2)-added samples. It was observed that sample x = 0.4 with a Y-123 phase percentage of 95.8% gives the highest T(c), smallest ∆T(c), and the sharpest diamagnetic transition in the normalised susceptibility curves. The microstructure also showed an excess of Sn precipitates on the sample’s surface at x = 0.8 and above. As such, the best superconducting properties were observed at x = 0.4 SnO(2) addition inside the Y-123 host sample.
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spelling pubmed-63376482019-01-22 Structural and Superconducting Properties of Thermal Treatment-Synthesised Bulk YBa(2)Cu(3)O(7−δ) Superconductor: Effect of Addition of SnO(2) Nanoparticles Mohd Yusuf, Nur Nabilah Awang Kechik, Mohd Mustafa Baqiah, Hussein Soo Kien, Chen Kean Pah, Lim Shaari, Abdul Halim Wan Jusoh, Wan Nur Wathiq Abd Sukor, Safia Izzati Mousa Dihom, Mustafa Talib, Zainal Abidin Abd-Shukor, Roslan Materials (Basel) Article YBa(2)Cu(3)O(7−δ) (Y-123) bulk superconductors with the addition of (0.0, 0.2, 0.4, 0.6, 0.8, and 1.0 wt.%) SnO(2) nanoparticles were synthesised via a thermal treatment method. The influence of SnO(2) addition on the superconducting properties by means of critical temperature, T(c), AC susceptibility, phase formation and microstructures, including its elemental composition analysis, were studied. Sharp superconducting transition, ∆T(c), and diamagnetic transition were obtained for all SnO(2)-added samples. It was observed that sample x = 0.4 with a Y-123 phase percentage of 95.8% gives the highest T(c), smallest ∆T(c), and the sharpest diamagnetic transition in the normalised susceptibility curves. The microstructure also showed an excess of Sn precipitates on the sample’s surface at x = 0.8 and above. As such, the best superconducting properties were observed at x = 0.4 SnO(2) addition inside the Y-123 host sample. MDPI 2018-12-28 /pmc/articles/PMC6337648/ /pubmed/30597840 http://dx.doi.org/10.3390/ma12010092 Text en © 2018 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Mohd Yusuf, Nur Nabilah
Awang Kechik, Mohd Mustafa
Baqiah, Hussein
Soo Kien, Chen
Kean Pah, Lim
Shaari, Abdul Halim
Wan Jusoh, Wan Nur Wathiq
Abd Sukor, Safia Izzati
Mousa Dihom, Mustafa
Talib, Zainal Abidin
Abd-Shukor, Roslan
Structural and Superconducting Properties of Thermal Treatment-Synthesised Bulk YBa(2)Cu(3)O(7−δ) Superconductor: Effect of Addition of SnO(2) Nanoparticles
title Structural and Superconducting Properties of Thermal Treatment-Synthesised Bulk YBa(2)Cu(3)O(7−δ) Superconductor: Effect of Addition of SnO(2) Nanoparticles
title_full Structural and Superconducting Properties of Thermal Treatment-Synthesised Bulk YBa(2)Cu(3)O(7−δ) Superconductor: Effect of Addition of SnO(2) Nanoparticles
title_fullStr Structural and Superconducting Properties of Thermal Treatment-Synthesised Bulk YBa(2)Cu(3)O(7−δ) Superconductor: Effect of Addition of SnO(2) Nanoparticles
title_full_unstemmed Structural and Superconducting Properties of Thermal Treatment-Synthesised Bulk YBa(2)Cu(3)O(7−δ) Superconductor: Effect of Addition of SnO(2) Nanoparticles
title_short Structural and Superconducting Properties of Thermal Treatment-Synthesised Bulk YBa(2)Cu(3)O(7−δ) Superconductor: Effect of Addition of SnO(2) Nanoparticles
title_sort structural and superconducting properties of thermal treatment-synthesised bulk yba(2)cu(3)o(7−δ) superconductor: effect of addition of sno(2) nanoparticles
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6337648/
https://www.ncbi.nlm.nih.gov/pubmed/30597840
http://dx.doi.org/10.3390/ma12010092
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