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Structural and Superconducting Properties of Thermal Treatment-Synthesised Bulk YBa(2)Cu(3)O(7−δ) Superconductor: Effect of Addition of SnO(2) Nanoparticles
YBa(2)Cu(3)O(7−δ) (Y-123) bulk superconductors with the addition of (0.0, 0.2, 0.4, 0.6, 0.8, and 1.0 wt.%) SnO(2) nanoparticles were synthesised via a thermal treatment method. The influence of SnO(2) addition on the superconducting properties by means of critical temperature, T(c), AC susceptibili...
Autores principales: | , , , , , , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2018
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6337648/ https://www.ncbi.nlm.nih.gov/pubmed/30597840 http://dx.doi.org/10.3390/ma12010092 |
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author | Mohd Yusuf, Nur Nabilah Awang Kechik, Mohd Mustafa Baqiah, Hussein Soo Kien, Chen Kean Pah, Lim Shaari, Abdul Halim Wan Jusoh, Wan Nur Wathiq Abd Sukor, Safia Izzati Mousa Dihom, Mustafa Talib, Zainal Abidin Abd-Shukor, Roslan |
author_facet | Mohd Yusuf, Nur Nabilah Awang Kechik, Mohd Mustafa Baqiah, Hussein Soo Kien, Chen Kean Pah, Lim Shaari, Abdul Halim Wan Jusoh, Wan Nur Wathiq Abd Sukor, Safia Izzati Mousa Dihom, Mustafa Talib, Zainal Abidin Abd-Shukor, Roslan |
author_sort | Mohd Yusuf, Nur Nabilah |
collection | PubMed |
description | YBa(2)Cu(3)O(7−δ) (Y-123) bulk superconductors with the addition of (0.0, 0.2, 0.4, 0.6, 0.8, and 1.0 wt.%) SnO(2) nanoparticles were synthesised via a thermal treatment method. The influence of SnO(2) addition on the superconducting properties by means of critical temperature, T(c), AC susceptibility, phase formation and microstructures, including its elemental composition analysis, were studied. Sharp superconducting transition, ∆T(c), and diamagnetic transition were obtained for all SnO(2)-added samples. It was observed that sample x = 0.4 with a Y-123 phase percentage of 95.8% gives the highest T(c), smallest ∆T(c), and the sharpest diamagnetic transition in the normalised susceptibility curves. The microstructure also showed an excess of Sn precipitates on the sample’s surface at x = 0.8 and above. As such, the best superconducting properties were observed at x = 0.4 SnO(2) addition inside the Y-123 host sample. |
format | Online Article Text |
id | pubmed-6337648 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2018 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-63376482019-01-22 Structural and Superconducting Properties of Thermal Treatment-Synthesised Bulk YBa(2)Cu(3)O(7−δ) Superconductor: Effect of Addition of SnO(2) Nanoparticles Mohd Yusuf, Nur Nabilah Awang Kechik, Mohd Mustafa Baqiah, Hussein Soo Kien, Chen Kean Pah, Lim Shaari, Abdul Halim Wan Jusoh, Wan Nur Wathiq Abd Sukor, Safia Izzati Mousa Dihom, Mustafa Talib, Zainal Abidin Abd-Shukor, Roslan Materials (Basel) Article YBa(2)Cu(3)O(7−δ) (Y-123) bulk superconductors with the addition of (0.0, 0.2, 0.4, 0.6, 0.8, and 1.0 wt.%) SnO(2) nanoparticles were synthesised via a thermal treatment method. The influence of SnO(2) addition on the superconducting properties by means of critical temperature, T(c), AC susceptibility, phase formation and microstructures, including its elemental composition analysis, were studied. Sharp superconducting transition, ∆T(c), and diamagnetic transition were obtained for all SnO(2)-added samples. It was observed that sample x = 0.4 with a Y-123 phase percentage of 95.8% gives the highest T(c), smallest ∆T(c), and the sharpest diamagnetic transition in the normalised susceptibility curves. The microstructure also showed an excess of Sn precipitates on the sample’s surface at x = 0.8 and above. As such, the best superconducting properties were observed at x = 0.4 SnO(2) addition inside the Y-123 host sample. MDPI 2018-12-28 /pmc/articles/PMC6337648/ /pubmed/30597840 http://dx.doi.org/10.3390/ma12010092 Text en © 2018 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Mohd Yusuf, Nur Nabilah Awang Kechik, Mohd Mustafa Baqiah, Hussein Soo Kien, Chen Kean Pah, Lim Shaari, Abdul Halim Wan Jusoh, Wan Nur Wathiq Abd Sukor, Safia Izzati Mousa Dihom, Mustafa Talib, Zainal Abidin Abd-Shukor, Roslan Structural and Superconducting Properties of Thermal Treatment-Synthesised Bulk YBa(2)Cu(3)O(7−δ) Superconductor: Effect of Addition of SnO(2) Nanoparticles |
title | Structural and Superconducting Properties of Thermal Treatment-Synthesised Bulk YBa(2)Cu(3)O(7−δ) Superconductor: Effect of Addition of SnO(2) Nanoparticles |
title_full | Structural and Superconducting Properties of Thermal Treatment-Synthesised Bulk YBa(2)Cu(3)O(7−δ) Superconductor: Effect of Addition of SnO(2) Nanoparticles |
title_fullStr | Structural and Superconducting Properties of Thermal Treatment-Synthesised Bulk YBa(2)Cu(3)O(7−δ) Superconductor: Effect of Addition of SnO(2) Nanoparticles |
title_full_unstemmed | Structural and Superconducting Properties of Thermal Treatment-Synthesised Bulk YBa(2)Cu(3)O(7−δ) Superconductor: Effect of Addition of SnO(2) Nanoparticles |
title_short | Structural and Superconducting Properties of Thermal Treatment-Synthesised Bulk YBa(2)Cu(3)O(7−δ) Superconductor: Effect of Addition of SnO(2) Nanoparticles |
title_sort | structural and superconducting properties of thermal treatment-synthesised bulk yba(2)cu(3)o(7−δ) superconductor: effect of addition of sno(2) nanoparticles |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6337648/ https://www.ncbi.nlm.nih.gov/pubmed/30597840 http://dx.doi.org/10.3390/ma12010092 |
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