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Low-budget 3D-printed equipment for continuous flow reactions

This article describes the development and manufacturing of lab equipment, which is needed for the use in flow chemistry. We developed a rack of four syringe pumps controlled by one Arduino computer, which can be manufactured with a commonly available 3D printer and readily available parts. Also, we...

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Detalles Bibliográficos
Autores principales: Neumaier, Jochen M, Madani, Amiera, Klein, Thomas, Ziegler, Thomas
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Beilstein-Institut 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6404462/
https://www.ncbi.nlm.nih.gov/pubmed/30873240
http://dx.doi.org/10.3762/bjoc.15.50
Descripción
Sumario:This article describes the development and manufacturing of lab equipment, which is needed for the use in flow chemistry. We developed a rack of four syringe pumps controlled by one Arduino computer, which can be manufactured with a commonly available 3D printer and readily available parts. Also, we printed various flow reactor cells, which are fully customizable for each individual reaction. With this equipment we performed some multistep glycosylation reactions, where multiple 3D-printed flow reactors were used in series.