Low-budget 3D-printed equipment for continuous flow reactions

This article describes the development and manufacturing of lab equipment, which is needed for the use in flow chemistry. We developed a rack of four syringe pumps controlled by one Arduino computer, which can be manufactured with a commonly available 3D printer and readily available parts. Also, we...

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Autores principales: Neumaier, Jochen M, Madani, Amiera, Klein, Thomas, Ziegler, Thomas
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Beilstein-Institut 2019
Materias:
Full Research Paper
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6404462/
https://www.ncbi.nlm.nih.gov/pubmed/30873240
http://dx.doi.org/10.3762/bjoc.15.50
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author Neumaier, Jochen M
Madani, Amiera
Klein, Thomas
Ziegler, Thomas
author_facet Neumaier, Jochen M
Madani, Amiera
Klein, Thomas
Ziegler, Thomas
author_sort Neumaier, Jochen M
collection PubMed
description This article describes the development and manufacturing of lab equipment, which is needed for the use in flow chemistry. We developed a rack of four syringe pumps controlled by one Arduino computer, which can be manufactured with a commonly available 3D printer and readily available parts. Also, we printed various flow reactor cells, which are fully customizable for each individual reaction. With this equipment we performed some multistep glycosylation reactions, where multiple 3D-printed flow reactors were used in series.
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spelling pubmed-64044622019-03-14 Low-budget 3D-printed equipment for continuous flow reactions Neumaier, Jochen M Madani, Amiera Klein, Thomas Ziegler, Thomas Beilstein J Org Chem Full Research Paper This article describes the development and manufacturing of lab equipment, which is needed for the use in flow chemistry. We developed a rack of four syringe pumps controlled by one Arduino computer, which can be manufactured with a commonly available 3D printer and readily available parts. Also, we printed various flow reactor cells, which are fully customizable for each individual reaction. With this equipment we performed some multistep glycosylation reactions, where multiple 3D-printed flow reactors were used in series. Beilstein-Institut 2019-02-26 /pmc/articles/PMC6404462/ /pubmed/30873240 http://dx.doi.org/10.3762/bjoc.15.50 Text en Copyright © 2019, Neumaier et al. https://creativecommons.org/licenses/by/4.0https://www.beilstein-journals.org/bjoc/termsThis is an Open Access article under the terms of the Creative Commons Attribution License (https://creativecommons.org/licenses/by/4.0). Please note that the reuse, redistribution and reproduction in particular requires that the authors and source are credited. The license is subject to the Beilstein Journal of Organic Chemistry terms and conditions: (https://www.beilstein-journals.org/bjoc/terms)
spellingShingle Full Research Paper
Neumaier, Jochen M
Madani, Amiera
Klein, Thomas
Ziegler, Thomas
Low-budget 3D-printed equipment for continuous flow reactions
title Low-budget 3D-printed equipment for continuous flow reactions
title_full Low-budget 3D-printed equipment for continuous flow reactions
title_fullStr Low-budget 3D-printed equipment for continuous flow reactions
title_full_unstemmed Low-budget 3D-printed equipment for continuous flow reactions
title_short Low-budget 3D-printed equipment for continuous flow reactions
title_sort low-budget 3d-printed equipment for continuous flow reactions
topic Full Research Paper
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6404462/
https://www.ncbi.nlm.nih.gov/pubmed/30873240
http://dx.doi.org/10.3762/bjoc.15.50
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