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Rotatable precipitates change the scale-free to scale dependent statistics in compressed Ti nano-pillars

Compressed nano-pillars crackle from moving dislocations, which reduces plastic stability. Crackling noise is characterized by stress drops or strain bursts, which scale over a large region of sizes leading to power law statistics. Here we report that this “classic” behaviour is not valid in Ti-base...

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Autores principales: Pan, Yan, Wu, Haijun, Wang, Xiaofei, Sun, Qiaoyan, Xiao, Lin, Ding, Xiangdong, Sun, Jun, Salje, Ekhard K. H.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6405840/
https://www.ncbi.nlm.nih.gov/pubmed/30846841
http://dx.doi.org/10.1038/s41598-019-40526-5
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author Pan, Yan
Wu, Haijun
Wang, Xiaofei
Sun, Qiaoyan
Xiao, Lin
Ding, Xiangdong
Sun, Jun
Salje, Ekhard K. H.
author_facet Pan, Yan
Wu, Haijun
Wang, Xiaofei
Sun, Qiaoyan
Xiao, Lin
Ding, Xiangdong
Sun, Jun
Salje, Ekhard K. H.
author_sort Pan, Yan
collection PubMed
description Compressed nano-pillars crackle from moving dislocations, which reduces plastic stability. Crackling noise is characterized by stress drops or strain bursts, which scale over a large region of sizes leading to power law statistics. Here we report that this “classic” behaviour is not valid in Ti-based nanopillars for a counterintuitive reason: we tailor precipitates inside the nano-pillar, which “regulate” the flux of dislocations. It is not because the nano-pillars become too small to sustain large dislocation movements, the effect is hence independent of size. Our precipitates act as “rotors”: local stress initiates the rotation of inclusions, which reduces the stress amplitudes dramatically. The size distribution of stress drops simultaneously changes from power law to exponential. Rotors act like revolving doors limiting the number of passing dislocations. Hence each collapse becomes weak. We present experimental evidence for Ti-based nano-pillars (diameters between 300 nm and 2 μm) with power law distributions of crackling noise P(s) ∼ s(−τ) with τ ∼ 2 in the defect free or non-rotatable precipitate states. Rotors change the size distribution to P(s) ∼ exp(−s/s(0)). Rotors are inclusions of ω-phase that aligns under stress along slip planes and limit dislocation glide to small distances with high nucleation rates. This opens new ways to make nano-pillars more stable.
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spelling pubmed-64058402019-03-11 Rotatable precipitates change the scale-free to scale dependent statistics in compressed Ti nano-pillars Pan, Yan Wu, Haijun Wang, Xiaofei Sun, Qiaoyan Xiao, Lin Ding, Xiangdong Sun, Jun Salje, Ekhard K. H. Sci Rep Article Compressed nano-pillars crackle from moving dislocations, which reduces plastic stability. Crackling noise is characterized by stress drops or strain bursts, which scale over a large region of sizes leading to power law statistics. Here we report that this “classic” behaviour is not valid in Ti-based nanopillars for a counterintuitive reason: we tailor precipitates inside the nano-pillar, which “regulate” the flux of dislocations. It is not because the nano-pillars become too small to sustain large dislocation movements, the effect is hence independent of size. Our precipitates act as “rotors”: local stress initiates the rotation of inclusions, which reduces the stress amplitudes dramatically. The size distribution of stress drops simultaneously changes from power law to exponential. Rotors act like revolving doors limiting the number of passing dislocations. Hence each collapse becomes weak. We present experimental evidence for Ti-based nano-pillars (diameters between 300 nm and 2 μm) with power law distributions of crackling noise P(s) ∼ s(−τ) with τ ∼ 2 in the defect free or non-rotatable precipitate states. Rotors change the size distribution to P(s) ∼ exp(−s/s(0)). Rotors are inclusions of ω-phase that aligns under stress along slip planes and limit dislocation glide to small distances with high nucleation rates. This opens new ways to make nano-pillars more stable. Nature Publishing Group UK 2019-03-07 /pmc/articles/PMC6405840/ /pubmed/30846841 http://dx.doi.org/10.1038/s41598-019-40526-5 Text en © The Author(s) 2019 Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.
spellingShingle Article
Pan, Yan
Wu, Haijun
Wang, Xiaofei
Sun, Qiaoyan
Xiao, Lin
Ding, Xiangdong
Sun, Jun
Salje, Ekhard K. H.
Rotatable precipitates change the scale-free to scale dependent statistics in compressed Ti nano-pillars
title Rotatable precipitates change the scale-free to scale dependent statistics in compressed Ti nano-pillars
title_full Rotatable precipitates change the scale-free to scale dependent statistics in compressed Ti nano-pillars
title_fullStr Rotatable precipitates change the scale-free to scale dependent statistics in compressed Ti nano-pillars
title_full_unstemmed Rotatable precipitates change the scale-free to scale dependent statistics in compressed Ti nano-pillars
title_short Rotatable precipitates change the scale-free to scale dependent statistics in compressed Ti nano-pillars
title_sort rotatable precipitates change the scale-free to scale dependent statistics in compressed ti nano-pillars
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6405840/
https://www.ncbi.nlm.nih.gov/pubmed/30846841
http://dx.doi.org/10.1038/s41598-019-40526-5
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