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Evaluation of Band-Selective HSQC and HMBC: Methodological Validation on the Cyclosporin Cyclic Peptide and Application for Poly(3-hydroxyalkanoate)s Stereoregularity Determination

Band-selective (bs) HSQC, improving spectral resolution by restriction of the heteronuclear dimension without inducing spectral folding, has been recently used for polymer tacticity determination. Herein is reported an evaluation of various bs-HSQC and bs-HMBC sequences, first from a methodological...

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Detalles Bibliográficos
Autores principales: Caytan, Elsa, Ligny, Romain, Carpentier, Jean-François, Guillaume, Sophie M.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2018
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6415406/
https://www.ncbi.nlm.nih.gov/pubmed/30966567
http://dx.doi.org/10.3390/polym10050533