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Microstructures and Properties of Porous Liquid-Phase-Sintered SiC Ceramic by Hot Press Sintering

Porous liquid-phase-sintered SiC (L-SiC) ceramics were successfully fabricated by hot press sintering (HP) at 1800 °C in argon, using Al(2)O(3) and Y(2)O(3) as oxide additions. By varying the starting coarse SiC particle size, the relationships between pore microstructures and flexural strength as w...

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Detalles Bibliográficos
Autores principales: Li, Yajie, Wu, Haibo, Liu, Xuejian, Huang, Zhengren
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6416541/
https://www.ncbi.nlm.nih.gov/pubmed/30791627
http://dx.doi.org/10.3390/ma12040639
Descripción
Sumario:Porous liquid-phase-sintered SiC (L-SiC) ceramics were successfully fabricated by hot press sintering (HP) at 1800 °C in argon, using Al(2)O(3) and Y(2)O(3) as oxide additions. By varying the starting coarse SiC particle size, the relationships between pore microstructures and flexural strength as well as gas permeability of porous L-SiC were examined. All the as-sintered samples possessed homogeneous interconnected pores. The porosity of porous L-SiC decreased from 34.0% to 25.9%, and the peak pore size increased from 1.1 to 3.8 μm as the coarse SiC particle sizes increased. The flexural strengths of porous L-SiC ceramics at room temperature and 1000 °C were as high as 104.3 ± 7.3 MPa and 78.8 ± 5.1 MPa, respectively, though there was a decrease in accordance with their increasing pore sizes and particle sizes. Moreover, their gas permeability increased from 1.4 × 10(−14) m(2) to 4.6 × 10(−14) m(2) with the increase of pore size in spite of their decreased porosity.