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Mineralogical, Textural and Physical Characterisation to Determine Deterioration Susceptibility of Irulegi Castle Lime Mortars (Navarre, Spain)

Archaeological lime mortars from the Tower Keep and West perimeter wall of Irulegi Castle (Navarre, Spain) were analysed to determine susceptibility to deterioration. Chemical, mineralogical, textural and physical characterisation was performed by different tests and multianalysis techniques in orde...

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Autores principales: Ponce-Antón, Graciela, Arizzi, Anna, Zuluaga, Maria Cruz, Cultrone, Giuseppe, Ortega, Luis Angel, Agirre Mauleon, Juantxo
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6416602/
https://www.ncbi.nlm.nih.gov/pubmed/30781373
http://dx.doi.org/10.3390/ma12040584
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author Ponce-Antón, Graciela
Arizzi, Anna
Zuluaga, Maria Cruz
Cultrone, Giuseppe
Ortega, Luis Angel
Agirre Mauleon, Juantxo
author_facet Ponce-Antón, Graciela
Arizzi, Anna
Zuluaga, Maria Cruz
Cultrone, Giuseppe
Ortega, Luis Angel
Agirre Mauleon, Juantxo
author_sort Ponce-Antón, Graciela
collection PubMed
description Archaeological lime mortars from the Tower Keep and West perimeter wall of Irulegi Castle (Navarre, Spain) were analysed to determine susceptibility to deterioration. Chemical, mineralogical, textural and physical characterisation was performed by different tests and multianalysis techniques in order to determine the intrinsic features of the original historical mortars at the castle. Samples from the Tower Keep are more prone to deteriorate compared with the West perimeter wall due to high water absorption capacity and high porosity. A high degree of pore interconnection, high desorption index and the presence of high pore volume in the 0.01 to 1 µm size range affect the mortar durability since pores retain water longer inside the mortar. Local environment conditions with persistent annual rainfall, high humidity and temperature variations contribute to the decay process of the original mortar. Characterisation of historical mortars not only allows better understanding of susceptibility to deterioration but also helps the design of compatible and durable repair mortar for future interventions on historical heritage. Compatibility of new materials with the historical mortar will be ensured by studying mortar characteristics and properties.
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spelling pubmed-64166022019-03-29 Mineralogical, Textural and Physical Characterisation to Determine Deterioration Susceptibility of Irulegi Castle Lime Mortars (Navarre, Spain) Ponce-Antón, Graciela Arizzi, Anna Zuluaga, Maria Cruz Cultrone, Giuseppe Ortega, Luis Angel Agirre Mauleon, Juantxo Materials (Basel) Article Archaeological lime mortars from the Tower Keep and West perimeter wall of Irulegi Castle (Navarre, Spain) were analysed to determine susceptibility to deterioration. Chemical, mineralogical, textural and physical characterisation was performed by different tests and multianalysis techniques in order to determine the intrinsic features of the original historical mortars at the castle. Samples from the Tower Keep are more prone to deteriorate compared with the West perimeter wall due to high water absorption capacity and high porosity. A high degree of pore interconnection, high desorption index and the presence of high pore volume in the 0.01 to 1 µm size range affect the mortar durability since pores retain water longer inside the mortar. Local environment conditions with persistent annual rainfall, high humidity and temperature variations contribute to the decay process of the original mortar. Characterisation of historical mortars not only allows better understanding of susceptibility to deterioration but also helps the design of compatible and durable repair mortar for future interventions on historical heritage. Compatibility of new materials with the historical mortar will be ensured by studying mortar characteristics and properties. MDPI 2019-02-15 /pmc/articles/PMC6416602/ /pubmed/30781373 http://dx.doi.org/10.3390/ma12040584 Text en © 2019 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Ponce-Antón, Graciela
Arizzi, Anna
Zuluaga, Maria Cruz
Cultrone, Giuseppe
Ortega, Luis Angel
Agirre Mauleon, Juantxo
Mineralogical, Textural and Physical Characterisation to Determine Deterioration Susceptibility of Irulegi Castle Lime Mortars (Navarre, Spain)
title Mineralogical, Textural and Physical Characterisation to Determine Deterioration Susceptibility of Irulegi Castle Lime Mortars (Navarre, Spain)
title_full Mineralogical, Textural and Physical Characterisation to Determine Deterioration Susceptibility of Irulegi Castle Lime Mortars (Navarre, Spain)
title_fullStr Mineralogical, Textural and Physical Characterisation to Determine Deterioration Susceptibility of Irulegi Castle Lime Mortars (Navarre, Spain)
title_full_unstemmed Mineralogical, Textural and Physical Characterisation to Determine Deterioration Susceptibility of Irulegi Castle Lime Mortars (Navarre, Spain)
title_short Mineralogical, Textural and Physical Characterisation to Determine Deterioration Susceptibility of Irulegi Castle Lime Mortars (Navarre, Spain)
title_sort mineralogical, textural and physical characterisation to determine deterioration susceptibility of irulegi castle lime mortars (navarre, spain)
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6416602/
https://www.ncbi.nlm.nih.gov/pubmed/30781373
http://dx.doi.org/10.3390/ma12040584
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