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Synthesis and Characterization of TiO(2)-ZnO-MgO Mixed Oxide and Their Antibacterial Activity

TiO(2)-ZnO-MgO mixed oxide nanomaterials (MONs) were synthetized via the sol-gel method and characterized by scanning electron microscopy (SEM) coupled with energy dispersive spectroscopy (EDS), transmission electron microscopy (TEM), nitrogen physisorption analysis, X-ray diffraction (XRD), UV-Vis...

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Autores principales: Anaya-Esparza, Luis M., Montalvo-González, Efigenia, González-Silva, Napoleón, Méndez-Robles, María D., Romero-Toledo, Rafael, Yahia, Elhadi M., Pérez-Larios, Alejandro
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6427488/
https://www.ncbi.nlm.nih.gov/pubmed/30818789
http://dx.doi.org/10.3390/ma12050698
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author Anaya-Esparza, Luis M.
Montalvo-González, Efigenia
González-Silva, Napoleón
Méndez-Robles, María D.
Romero-Toledo, Rafael
Yahia, Elhadi M.
Pérez-Larios, Alejandro
author_facet Anaya-Esparza, Luis M.
Montalvo-González, Efigenia
González-Silva, Napoleón
Méndez-Robles, María D.
Romero-Toledo, Rafael
Yahia, Elhadi M.
Pérez-Larios, Alejandro
author_sort Anaya-Esparza, Luis M.
collection PubMed
description TiO(2)-ZnO-MgO mixed oxide nanomaterials (MONs) were synthetized via the sol-gel method and characterized by scanning electron microscopy (SEM) coupled with energy dispersive spectroscopy (EDS), transmission electron microscopy (TEM), nitrogen physisorption analysis, X-ray diffraction (XRD), UV-Vis diffuse reflectance spectroscopy (UV-Vis DRS), Fourier transform infrared spectroscopy (FTIR), and color (Luminosity (L), a, b, Chrome, hue) parameters. Furthermore, the antimicrobial activity of the MONs was tested against Escherichia coli (EC), Salmonella paratyphi (SP), Staphylococcus aureus (SA), and Listeria monocytogenes (LM). The MONs presented a semi globular-ovoid shape of ≤100 nm. Samples were classified as mesoporous materials and preserved in the TiO(2) anatase phase, with slight changes in the color parameters of the MONs in comparison with pure TiO(2). The MONs exhibited antimicrobial activity, and their effect on the tested bacteria was in the following order: EC > SP > SA > LM. Therefore, MONs could be used as antimicrobial agents for industrial applications.
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spelling pubmed-64274882019-04-15 Synthesis and Characterization of TiO(2)-ZnO-MgO Mixed Oxide and Their Antibacterial Activity Anaya-Esparza, Luis M. Montalvo-González, Efigenia González-Silva, Napoleón Méndez-Robles, María D. Romero-Toledo, Rafael Yahia, Elhadi M. Pérez-Larios, Alejandro Materials (Basel) Article TiO(2)-ZnO-MgO mixed oxide nanomaterials (MONs) were synthetized via the sol-gel method and characterized by scanning electron microscopy (SEM) coupled with energy dispersive spectroscopy (EDS), transmission electron microscopy (TEM), nitrogen physisorption analysis, X-ray diffraction (XRD), UV-Vis diffuse reflectance spectroscopy (UV-Vis DRS), Fourier transform infrared spectroscopy (FTIR), and color (Luminosity (L), a, b, Chrome, hue) parameters. Furthermore, the antimicrobial activity of the MONs was tested against Escherichia coli (EC), Salmonella paratyphi (SP), Staphylococcus aureus (SA), and Listeria monocytogenes (LM). The MONs presented a semi globular-ovoid shape of ≤100 nm. Samples were classified as mesoporous materials and preserved in the TiO(2) anatase phase, with slight changes in the color parameters of the MONs in comparison with pure TiO(2). The MONs exhibited antimicrobial activity, and their effect on the tested bacteria was in the following order: EC > SP > SA > LM. Therefore, MONs could be used as antimicrobial agents for industrial applications. MDPI 2019-02-27 /pmc/articles/PMC6427488/ /pubmed/30818789 http://dx.doi.org/10.3390/ma12050698 Text en © 2019 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Anaya-Esparza, Luis M.
Montalvo-González, Efigenia
González-Silva, Napoleón
Méndez-Robles, María D.
Romero-Toledo, Rafael
Yahia, Elhadi M.
Pérez-Larios, Alejandro
Synthesis and Characterization of TiO(2)-ZnO-MgO Mixed Oxide and Their Antibacterial Activity
title Synthesis and Characterization of TiO(2)-ZnO-MgO Mixed Oxide and Their Antibacterial Activity
title_full Synthesis and Characterization of TiO(2)-ZnO-MgO Mixed Oxide and Their Antibacterial Activity
title_fullStr Synthesis and Characterization of TiO(2)-ZnO-MgO Mixed Oxide and Their Antibacterial Activity
title_full_unstemmed Synthesis and Characterization of TiO(2)-ZnO-MgO Mixed Oxide and Their Antibacterial Activity
title_short Synthesis and Characterization of TiO(2)-ZnO-MgO Mixed Oxide and Their Antibacterial Activity
title_sort synthesis and characterization of tio(2)-zno-mgo mixed oxide and their antibacterial activity
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6427488/
https://www.ncbi.nlm.nih.gov/pubmed/30818789
http://dx.doi.org/10.3390/ma12050698
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