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Magnetic Polyamide Nanocomposites for the Microextraction of Benzophenones from Water Samples

In this article, the influence of the monomers on the extraction efficiency and the effect of the addition of surfactants during the synthesis have also been considered. The sorption capacity of the resulting nanocomposites has been evaluated, in the dispersive micro-solid phase extraction format, b...

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Autores principales: Ghambari, Hoda, Reyes-Gallardo, Emilia M., Lucena, Rafael, Saraji, Mohammad, Cárdenas, Soledad
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6429122/
https://www.ncbi.nlm.nih.gov/pubmed/30857139
http://dx.doi.org/10.3390/molecules24050953
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author Ghambari, Hoda
Reyes-Gallardo, Emilia M.
Lucena, Rafael
Saraji, Mohammad
Cárdenas, Soledad
author_facet Ghambari, Hoda
Reyes-Gallardo, Emilia M.
Lucena, Rafael
Saraji, Mohammad
Cárdenas, Soledad
author_sort Ghambari, Hoda
collection PubMed
description In this article, the influence of the monomers on the extraction efficiency and the effect of the addition of surfactants during the synthesis have also been considered. The sorption capacity of the resulting nanocomposites has been evaluated, in the dispersive micro-solid phase extraction format, by determining that of six benzophenones in water using ultra performance liquid chromatography (UPLC) combined with photodiode array detection. Under the optimum conditions, the limits of detection were in the range of 0.5–4.3 ng/mL and the repeatability, expressed as the relative standard deviation (RSD), varied between 1.5% and 5.6%. The proposed method has been applied for the analysis of real water samples, providing relative recoveries in the interval of 84–105%
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spelling pubmed-64291222019-04-15 Magnetic Polyamide Nanocomposites for the Microextraction of Benzophenones from Water Samples Ghambari, Hoda Reyes-Gallardo, Emilia M. Lucena, Rafael Saraji, Mohammad Cárdenas, Soledad Molecules Article In this article, the influence of the monomers on the extraction efficiency and the effect of the addition of surfactants during the synthesis have also been considered. The sorption capacity of the resulting nanocomposites has been evaluated, in the dispersive micro-solid phase extraction format, by determining that of six benzophenones in water using ultra performance liquid chromatography (UPLC) combined with photodiode array detection. Under the optimum conditions, the limits of detection were in the range of 0.5–4.3 ng/mL and the repeatability, expressed as the relative standard deviation (RSD), varied between 1.5% and 5.6%. The proposed method has been applied for the analysis of real water samples, providing relative recoveries in the interval of 84–105% MDPI 2019-03-08 /pmc/articles/PMC6429122/ /pubmed/30857139 http://dx.doi.org/10.3390/molecules24050953 Text en © 2019 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Ghambari, Hoda
Reyes-Gallardo, Emilia M.
Lucena, Rafael
Saraji, Mohammad
Cárdenas, Soledad
Magnetic Polyamide Nanocomposites for the Microextraction of Benzophenones from Water Samples
title Magnetic Polyamide Nanocomposites for the Microextraction of Benzophenones from Water Samples
title_full Magnetic Polyamide Nanocomposites for the Microextraction of Benzophenones from Water Samples
title_fullStr Magnetic Polyamide Nanocomposites for the Microextraction of Benzophenones from Water Samples
title_full_unstemmed Magnetic Polyamide Nanocomposites for the Microextraction of Benzophenones from Water Samples
title_short Magnetic Polyamide Nanocomposites for the Microextraction of Benzophenones from Water Samples
title_sort magnetic polyamide nanocomposites for the microextraction of benzophenones from water samples
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6429122/
https://www.ncbi.nlm.nih.gov/pubmed/30857139
http://dx.doi.org/10.3390/molecules24050953
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