Cargando…
Magnetic Polyamide Nanocomposites for the Microextraction of Benzophenones from Water Samples
In this article, the influence of the monomers on the extraction efficiency and the effect of the addition of surfactants during the synthesis have also been considered. The sorption capacity of the resulting nanocomposites has been evaluated, in the dispersive micro-solid phase extraction format, b...
Autores principales: | , , , , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2019
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6429122/ https://www.ncbi.nlm.nih.gov/pubmed/30857139 http://dx.doi.org/10.3390/molecules24050953 |
_version_ | 1783405524227719168 |
---|---|
author | Ghambari, Hoda Reyes-Gallardo, Emilia M. Lucena, Rafael Saraji, Mohammad Cárdenas, Soledad |
author_facet | Ghambari, Hoda Reyes-Gallardo, Emilia M. Lucena, Rafael Saraji, Mohammad Cárdenas, Soledad |
author_sort | Ghambari, Hoda |
collection | PubMed |
description | In this article, the influence of the monomers on the extraction efficiency and the effect of the addition of surfactants during the synthesis have also been considered. The sorption capacity of the resulting nanocomposites has been evaluated, in the dispersive micro-solid phase extraction format, by determining that of six benzophenones in water using ultra performance liquid chromatography (UPLC) combined with photodiode array detection. Under the optimum conditions, the limits of detection were in the range of 0.5–4.3 ng/mL and the repeatability, expressed as the relative standard deviation (RSD), varied between 1.5% and 5.6%. The proposed method has been applied for the analysis of real water samples, providing relative recoveries in the interval of 84–105% |
format | Online Article Text |
id | pubmed-6429122 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2019 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-64291222019-04-15 Magnetic Polyamide Nanocomposites for the Microextraction of Benzophenones from Water Samples Ghambari, Hoda Reyes-Gallardo, Emilia M. Lucena, Rafael Saraji, Mohammad Cárdenas, Soledad Molecules Article In this article, the influence of the monomers on the extraction efficiency and the effect of the addition of surfactants during the synthesis have also been considered. The sorption capacity of the resulting nanocomposites has been evaluated, in the dispersive micro-solid phase extraction format, by determining that of six benzophenones in water using ultra performance liquid chromatography (UPLC) combined with photodiode array detection. Under the optimum conditions, the limits of detection were in the range of 0.5–4.3 ng/mL and the repeatability, expressed as the relative standard deviation (RSD), varied between 1.5% and 5.6%. The proposed method has been applied for the analysis of real water samples, providing relative recoveries in the interval of 84–105% MDPI 2019-03-08 /pmc/articles/PMC6429122/ /pubmed/30857139 http://dx.doi.org/10.3390/molecules24050953 Text en © 2019 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Ghambari, Hoda Reyes-Gallardo, Emilia M. Lucena, Rafael Saraji, Mohammad Cárdenas, Soledad Magnetic Polyamide Nanocomposites for the Microextraction of Benzophenones from Water Samples |
title | Magnetic Polyamide Nanocomposites for the Microextraction of Benzophenones from Water Samples |
title_full | Magnetic Polyamide Nanocomposites for the Microextraction of Benzophenones from Water Samples |
title_fullStr | Magnetic Polyamide Nanocomposites for the Microextraction of Benzophenones from Water Samples |
title_full_unstemmed | Magnetic Polyamide Nanocomposites for the Microextraction of Benzophenones from Water Samples |
title_short | Magnetic Polyamide Nanocomposites for the Microextraction of Benzophenones from Water Samples |
title_sort | magnetic polyamide nanocomposites for the microextraction of benzophenones from water samples |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6429122/ https://www.ncbi.nlm.nih.gov/pubmed/30857139 http://dx.doi.org/10.3390/molecules24050953 |
work_keys_str_mv | AT ghambarihoda magneticpolyamidenanocompositesforthemicroextractionofbenzophenonesfromwatersamples AT reyesgallardoemiliam magneticpolyamidenanocompositesforthemicroextractionofbenzophenonesfromwatersamples AT lucenarafael magneticpolyamidenanocompositesforthemicroextractionofbenzophenonesfromwatersamples AT sarajimohammad magneticpolyamidenanocompositesforthemicroextractionofbenzophenonesfromwatersamples AT cardenassoledad magneticpolyamidenanocompositesforthemicroextractionofbenzophenonesfromwatersamples |