Free-film small-angle neutron scattering: a novel container-free in situ sample environment with minimized H/D exchange

The development of a container-free sample environment which is particularly well suited for in situ reaction studies of liquid samples by small-angle neutron scattering and related techniques is reported. Hydrogen exchange with the humidity from air is reduced by an encapsulating setup in a bag fil...

Descripción completa

Detalles Bibliográficos
Autores principales: Krauss, Sebastian W., Schweins, Ralf, Magerl, Andreas, Zobel, Mirijam
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2019
Materias:
Research Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6448684/
https://www.ncbi.nlm.nih.gov/pubmed/30996715
http://dx.doi.org/10.1107/S1600576719000906
_version_ 1783408722485182464
author Krauss, Sebastian W.
Schweins, Ralf
Magerl, Andreas
Zobel, Mirijam
author_facet Krauss, Sebastian W.
Schweins, Ralf
Magerl, Andreas
Zobel, Mirijam
author_sort Krauss, Sebastian W.
collection PubMed
description The development of a container-free sample environment which is particularly well suited for in situ reaction studies of liquid samples by small-angle neutron scattering and related techniques is reported. Hydrogen exchange with the humidity from air is reduced by an encapsulating setup in a bag filled with an inert gas such as He. The effectiveness of this measure is quantitatively accessed by infrared absorption and gravimetry, and further correlated with neutron scattering.
format Online
Article
Text
id pubmed-6448684
institution National Center for Biotechnology Information
language English
publishDate 2019
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-64486842019-04-17 Free-film small-angle neutron scattering: a novel container-free in situ sample environment with minimized H/D exchange Krauss, Sebastian W. Schweins, Ralf Magerl, Andreas Zobel, Mirijam J Appl Crystallogr Research Papers The development of a container-free sample environment which is particularly well suited for in situ reaction studies of liquid samples by small-angle neutron scattering and related techniques is reported. Hydrogen exchange with the humidity from air is reduced by an encapsulating setup in a bag filled with an inert gas such as He. The effectiveness of this measure is quantitatively accessed by infrared absorption and gravimetry, and further correlated with neutron scattering. International Union of Crystallography 2019-02-26 /pmc/articles/PMC6448684/ /pubmed/30996715 http://dx.doi.org/10.1107/S1600576719000906 Text en © Sebastian W. Krauss et al. 2019 http://creativecommons.org/licenses/by/4.0/ This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.http://creativecommons.org/licenses/by/4.0/
spellingShingle Research Papers
Krauss, Sebastian W.
Schweins, Ralf
Magerl, Andreas
Zobel, Mirijam
Free-film small-angle neutron scattering: a novel container-free in situ sample environment with minimized H/D exchange
title Free-film small-angle neutron scattering: a novel container-free in situ sample environment with minimized H/D exchange
title_full Free-film small-angle neutron scattering: a novel container-free in situ sample environment with minimized H/D exchange
title_fullStr Free-film small-angle neutron scattering: a novel container-free in situ sample environment with minimized H/D exchange
title_full_unstemmed Free-film small-angle neutron scattering: a novel container-free in situ sample environment with minimized H/D exchange
title_short Free-film small-angle neutron scattering: a novel container-free in situ sample environment with minimized H/D exchange
title_sort free-film small-angle neutron scattering: a novel container-free in situ sample environment with minimized h/d exchange
topic Research Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6448684/
https://www.ncbi.nlm.nih.gov/pubmed/30996715
http://dx.doi.org/10.1107/S1600576719000906
work_keys_str_mv AT krausssebastianw freefilmsmallangleneutronscatteringanovelcontainerfreeinsitusampleenvironmentwithminimizedhdexchange
AT schweinsralf freefilmsmallangleneutronscatteringanovelcontainerfreeinsitusampleenvironmentwithminimizedhdexchange
AT magerlandreas freefilmsmallangleneutronscatteringanovelcontainerfreeinsitusampleenvironmentwithminimizedhdexchange
AT zobelmirijam freefilmsmallangleneutronscatteringanovelcontainerfreeinsitusampleenvironmentwithminimizedhdexchange

Ejemplares similares