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Data on validation using accuracy profile of HPLC-UV method
The data presented are related to the article entitled “Six Sigma quality approach for HPLC-UV method optimization” Ibrahim et al., 2019. The raw data of HPLC analysis of ascorbic acid (AS), paracetamol (PA) and guaifenesin (GU) are presented. Calibration standards were prepared at six concentration...
Autores principales: | , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Elsevier
2019
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6449764/ https://www.ncbi.nlm.nih.gov/pubmed/30993157 http://dx.doi.org/10.1016/j.dib.2019.103877 |
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author | Ibrahim, Ahmed M. Hendawy, Hassan A.M. Hassan, Wafaa S. Shalaby, Abdalla El-sayed, Heba M. |
author_facet | Ibrahim, Ahmed M. Hendawy, Hassan A.M. Hassan, Wafaa S. Shalaby, Abdalla El-sayed, Heba M. |
author_sort | Ibrahim, Ahmed M. |
collection | PubMed |
description | The data presented are related to the article entitled “Six Sigma quality approach for HPLC-UV method optimization” Ibrahim et al., 2019. The raw data of HPLC analysis of ascorbic acid (AS), paracetamol (PA) and guaifenesin (GU) are presented. Calibration standards were prepared at six concentrations levels (25%, 50%, 75%, 100%, 125% and 150%) each day and measured in triplicate. Validation standards were prepared at four concentration levels (25%, 60%, 100% and 150%) each day and measured in quintet. Three different series were used for method validation and prepared at the rate of one series per day. |
format | Online Article Text |
id | pubmed-6449764 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2019 |
publisher | Elsevier |
record_format | MEDLINE/PubMed |
spelling | pubmed-64497642019-04-16 Data on validation using accuracy profile of HPLC-UV method Ibrahim, Ahmed M. Hendawy, Hassan A.M. Hassan, Wafaa S. Shalaby, Abdalla El-sayed, Heba M. Data Brief Chemistry The data presented are related to the article entitled “Six Sigma quality approach for HPLC-UV method optimization” Ibrahim et al., 2019. The raw data of HPLC analysis of ascorbic acid (AS), paracetamol (PA) and guaifenesin (GU) are presented. Calibration standards were prepared at six concentrations levels (25%, 50%, 75%, 100%, 125% and 150%) each day and measured in triplicate. Validation standards were prepared at four concentration levels (25%, 60%, 100% and 150%) each day and measured in quintet. Three different series were used for method validation and prepared at the rate of one series per day. Elsevier 2019-03-26 /pmc/articles/PMC6449764/ /pubmed/30993157 http://dx.doi.org/10.1016/j.dib.2019.103877 Text en © 2019 The Authors http://creativecommons.org/licenses/by/4.0/ This is an open access article under the CC BY license (http://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Chemistry Ibrahim, Ahmed M. Hendawy, Hassan A.M. Hassan, Wafaa S. Shalaby, Abdalla El-sayed, Heba M. Data on validation using accuracy profile of HPLC-UV method |
title | Data on validation using accuracy profile of HPLC-UV method |
title_full | Data on validation using accuracy profile of HPLC-UV method |
title_fullStr | Data on validation using accuracy profile of HPLC-UV method |
title_full_unstemmed | Data on validation using accuracy profile of HPLC-UV method |
title_short | Data on validation using accuracy profile of HPLC-UV method |
title_sort | data on validation using accuracy profile of hplc-uv method |
topic | Chemistry |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6449764/ https://www.ncbi.nlm.nih.gov/pubmed/30993157 http://dx.doi.org/10.1016/j.dib.2019.103877 |
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