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Inline Reaction Monitoring of Amine-Catalyzed Acetylation of Benzyl Alcohol Using a Microfluidic Stripline Nuclear Magnetic Resonance Setup
[Image: see text] We present an in-depth study of the acetylation of benzyl alcohol in the presence of N,N-diisopropylethylamine (DIPEA) by nuclear magnetic resonance (NMR) monitoring of the reaction from 1.5 s to several minutes. We have adapted the NMR setup to be compatible to microreactor techno...
Autores principales: | Oosthoek-de Vries, Anna Jo, Nieuwland, Pieter J., Bart, Jacob, Koch, Kaspar, Janssen, Johannes W. G., van Bentum, P. Jan M., Rutjes, Floris P. J. T., Gardeniers, Han J. G. E., Kentgens, Arno P. M. |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
American Chemical
Society
2019
|
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6449804/ https://www.ncbi.nlm.nih.gov/pubmed/30864795 http://dx.doi.org/10.1021/jacs.9b00039 |
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