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Characterizing Complex Mineral Structures in Thin Sections of Geological Samples with a Scanning Hall Effect Microscope

We improved a magnetic scanning microscope for measuring the magnetic properties of minerals in thin sections of geological samples at submillimeter scales. The microscope is comprised of a 200 µm diameter Hall sensor that is located at a distance of 142 µm from the sample; an electromagnet capable...

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Autores principales: Araujo, Jefferson F. D. F., Reis, Andre L. A., Oliveira, Vanderlei C., Santos, Amanda F., Luz-Lima, Cleanio, Yokoyama, Elder, Mendoza, Leonardo A. F., Pereira, João M. B., Bruno, Antonio C.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6479408/
https://www.ncbi.nlm.nih.gov/pubmed/30959784
http://dx.doi.org/10.3390/s19071636
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author Araujo, Jefferson F. D. F.
Reis, Andre L. A.
Oliveira, Vanderlei C.
Santos, Amanda F.
Luz-Lima, Cleanio
Yokoyama, Elder
Mendoza, Leonardo A. F.
Pereira, João M. B.
Bruno, Antonio C.
author_facet Araujo, Jefferson F. D. F.
Reis, Andre L. A.
Oliveira, Vanderlei C.
Santos, Amanda F.
Luz-Lima, Cleanio
Yokoyama, Elder
Mendoza, Leonardo A. F.
Pereira, João M. B.
Bruno, Antonio C.
author_sort Araujo, Jefferson F. D. F.
collection PubMed
description We improved a magnetic scanning microscope for measuring the magnetic properties of minerals in thin sections of geological samples at submillimeter scales. The microscope is comprised of a 200 µm diameter Hall sensor that is located at a distance of 142 µm from the sample; an electromagnet capable of applying up to 500 mT DC magnetic fields to the sample over a 40 mm diameter region; a second Hall sensor arranged in a gradiometric configuration to cancel the background signal applied by the electromagnet and reduce the overall noise in the system; a custom-designed electronics system to bias the sensors and allow adjustments to the background signal cancelation; and a scanning XY stage with micrometer resolution. Our system achieves a spatial resolution of 200 µm with a noise at 6.0 Hz of 300 nT(rms)/(Hz)(1/2) in an unshielded environment. The magnetic moment sensitivity is 1.3 × 10(−11) Am(2). We successfully measured the representative magnetization of a geological sample using an alternative model that takes the sample geometry into account and identified different micrometric characteristics in the sample slice.
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spelling pubmed-64794082019-04-29 Characterizing Complex Mineral Structures in Thin Sections of Geological Samples with a Scanning Hall Effect Microscope Araujo, Jefferson F. D. F. Reis, Andre L. A. Oliveira, Vanderlei C. Santos, Amanda F. Luz-Lima, Cleanio Yokoyama, Elder Mendoza, Leonardo A. F. Pereira, João M. B. Bruno, Antonio C. Sensors (Basel) Article We improved a magnetic scanning microscope for measuring the magnetic properties of minerals in thin sections of geological samples at submillimeter scales. The microscope is comprised of a 200 µm diameter Hall sensor that is located at a distance of 142 µm from the sample; an electromagnet capable of applying up to 500 mT DC magnetic fields to the sample over a 40 mm diameter region; a second Hall sensor arranged in a gradiometric configuration to cancel the background signal applied by the electromagnet and reduce the overall noise in the system; a custom-designed electronics system to bias the sensors and allow adjustments to the background signal cancelation; and a scanning XY stage with micrometer resolution. Our system achieves a spatial resolution of 200 µm with a noise at 6.0 Hz of 300 nT(rms)/(Hz)(1/2) in an unshielded environment. The magnetic moment sensitivity is 1.3 × 10(−11) Am(2). We successfully measured the representative magnetization of a geological sample using an alternative model that takes the sample geometry into account and identified different micrometric characteristics in the sample slice. MDPI 2019-04-05 /pmc/articles/PMC6479408/ /pubmed/30959784 http://dx.doi.org/10.3390/s19071636 Text en © 2019 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Araujo, Jefferson F. D. F.
Reis, Andre L. A.
Oliveira, Vanderlei C.
Santos, Amanda F.
Luz-Lima, Cleanio
Yokoyama, Elder
Mendoza, Leonardo A. F.
Pereira, João M. B.
Bruno, Antonio C.
Characterizing Complex Mineral Structures in Thin Sections of Geological Samples with a Scanning Hall Effect Microscope
title Characterizing Complex Mineral Structures in Thin Sections of Geological Samples with a Scanning Hall Effect Microscope
title_full Characterizing Complex Mineral Structures in Thin Sections of Geological Samples with a Scanning Hall Effect Microscope
title_fullStr Characterizing Complex Mineral Structures in Thin Sections of Geological Samples with a Scanning Hall Effect Microscope
title_full_unstemmed Characterizing Complex Mineral Structures in Thin Sections of Geological Samples with a Scanning Hall Effect Microscope
title_short Characterizing Complex Mineral Structures in Thin Sections of Geological Samples with a Scanning Hall Effect Microscope
title_sort characterizing complex mineral structures in thin sections of geological samples with a scanning hall effect microscope
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6479408/
https://www.ncbi.nlm.nih.gov/pubmed/30959784
http://dx.doi.org/10.3390/s19071636
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