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Microstructure and Hot Deformation Behavior of Twin Roll Cast Mg-2Zn-1Al-0.3Ca Alloy

In the present work, the microstructure, texture, mechanical properties as well as hot deformation behavior of a Mg-2Zn-1Al-0.3Ca sheet manufactured by twin roll casting were investigated. The twin roll cast state reveals a dendritic microstructure with intermetallic compounds predominantly located...

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Autores principales: Kittner, Kristina, Ullmann, Madlen, Henseler, Thorsten, Kawalla, Rudolf, Prahl, Ulrich
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6479906/
https://www.ncbi.nlm.nih.gov/pubmed/30925661
http://dx.doi.org/10.3390/ma12071020
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author Kittner, Kristina
Ullmann, Madlen
Henseler, Thorsten
Kawalla, Rudolf
Prahl, Ulrich
author_facet Kittner, Kristina
Ullmann, Madlen
Henseler, Thorsten
Kawalla, Rudolf
Prahl, Ulrich
author_sort Kittner, Kristina
collection PubMed
description In the present work, the microstructure, texture, mechanical properties as well as hot deformation behavior of a Mg-2Zn-1Al-0.3Ca sheet manufactured by twin roll casting were investigated. The twin roll cast state reveals a dendritic microstructure with intermetallic compounds predominantly located in the interdendritic areas. The twin roll cast samples were annealed at 420 °C for 2 h followed by plane strain compression tests in order to study the hardening and softening behavior. Annealing treatment leads to the formation of a grain structure, consisting of equiaxed grains with an average diameter of approximately 19 µm. The twin roll cast state reveals a typical basal texture and the annealed state shows a weakened texture, by spreading basal poles along the transverse direction. The twin roll cast Mg-2Zn-1Al-0.3Ca alloy offers a good ultimate tensile strength of 240 MPa. The course of the flow curves indicate that dynamic recrystallization occurs during hot deformation. For the validity range from 250 °C to 450 °C as well as equivalent logarithmic strain rates from 0.01 s(−1) to 10 s(−1) calculated model coefficients are shown. The average activation energy for plastic flow of the twin roll cast and annealed Mg-2Zn-1Al-0.3Ca alloy amounts to 180.5 kJ/mol. The processing map reveals one domain with flow instability at temperatures above 370 °C and strain rates ranging from 3 s(−1) to 10 s(−1). Under these forming conditions, intergranular cracks arose and grew along the grain boundaries.
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spelling pubmed-64799062019-04-29 Microstructure and Hot Deformation Behavior of Twin Roll Cast Mg-2Zn-1Al-0.3Ca Alloy Kittner, Kristina Ullmann, Madlen Henseler, Thorsten Kawalla, Rudolf Prahl, Ulrich Materials (Basel) Article In the present work, the microstructure, texture, mechanical properties as well as hot deformation behavior of a Mg-2Zn-1Al-0.3Ca sheet manufactured by twin roll casting were investigated. The twin roll cast state reveals a dendritic microstructure with intermetallic compounds predominantly located in the interdendritic areas. The twin roll cast samples were annealed at 420 °C for 2 h followed by plane strain compression tests in order to study the hardening and softening behavior. Annealing treatment leads to the formation of a grain structure, consisting of equiaxed grains with an average diameter of approximately 19 µm. The twin roll cast state reveals a typical basal texture and the annealed state shows a weakened texture, by spreading basal poles along the transverse direction. The twin roll cast Mg-2Zn-1Al-0.3Ca alloy offers a good ultimate tensile strength of 240 MPa. The course of the flow curves indicate that dynamic recrystallization occurs during hot deformation. For the validity range from 250 °C to 450 °C as well as equivalent logarithmic strain rates from 0.01 s(−1) to 10 s(−1) calculated model coefficients are shown. The average activation energy for plastic flow of the twin roll cast and annealed Mg-2Zn-1Al-0.3Ca alloy amounts to 180.5 kJ/mol. The processing map reveals one domain with flow instability at temperatures above 370 °C and strain rates ranging from 3 s(−1) to 10 s(−1). Under these forming conditions, intergranular cracks arose and grew along the grain boundaries. MDPI 2019-03-28 /pmc/articles/PMC6479906/ /pubmed/30925661 http://dx.doi.org/10.3390/ma12071020 Text en © 2019 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Kittner, Kristina
Ullmann, Madlen
Henseler, Thorsten
Kawalla, Rudolf
Prahl, Ulrich
Microstructure and Hot Deformation Behavior of Twin Roll Cast Mg-2Zn-1Al-0.3Ca Alloy
title Microstructure and Hot Deformation Behavior of Twin Roll Cast Mg-2Zn-1Al-0.3Ca Alloy
title_full Microstructure and Hot Deformation Behavior of Twin Roll Cast Mg-2Zn-1Al-0.3Ca Alloy
title_fullStr Microstructure and Hot Deformation Behavior of Twin Roll Cast Mg-2Zn-1Al-0.3Ca Alloy
title_full_unstemmed Microstructure and Hot Deformation Behavior of Twin Roll Cast Mg-2Zn-1Al-0.3Ca Alloy
title_short Microstructure and Hot Deformation Behavior of Twin Roll Cast Mg-2Zn-1Al-0.3Ca Alloy
title_sort microstructure and hot deformation behavior of twin roll cast mg-2zn-1al-0.3ca alloy
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6479906/
https://www.ncbi.nlm.nih.gov/pubmed/30925661
http://dx.doi.org/10.3390/ma12071020
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