Crystal structure of 4-(2-hy­droxy-3-meth­oxy­benzyl­amino)­benzoic acid di­methyl­formamide monosolvate monohydrate

The title compound, C(15)H(15)NO(4)·C(3)H(7)NO·H(2)O, a secondary amine mol­ecule, is accompanied by one equivalent of water and one equivalent of di­methyl­formamide (DMF) as solvents. The mol­ecule is non-planar, with a C(ar­yl)—CH(2)—NH—C(ar­yl) torsion angle of −66.3 (3)°. In the crystal, O—H⋯O...

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Detalles Bibliográficos
Autores principales: Faizi, Md. Serajul Haque, Kamaal, Saima, Ali, Arif, Ahmad, Musheer, Golenya, Irina A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2019
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6505596/
https://www.ncbi.nlm.nih.gov/pubmed/31110804
http://dx.doi.org/10.1107/S2056989019005103
Descripción
Sumario:The title compound, C(15)H(15)NO(4)·C(3)H(7)NO·H(2)O, a secondary amine mol­ecule, is accompanied by one equivalent of water and one equivalent of di­methyl­formamide (DMF) as solvents. The mol­ecule is non-planar, with a C(ar­yl)—CH(2)—NH—C(ar­yl) torsion angle of −66.3 (3)°. In the crystal, O—H⋯O and N—H⋯O hydrogen-bonding inter­actions between the amine mol­ecules and the two types of solvent mol­ecule result in the formation of a layered structure extending parallel to (010).

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