Crystal structure of 4-(2-hy­droxy-3-meth­oxy­benzyl­amino)­benzoic acid di­methyl­formamide monosolvate monohydrate

The title compound, C(15)H(15)NO(4)·C(3)H(7)NO·H(2)O, a secondary amine mol­ecule, is accompanied by one equivalent of water and one equivalent of di­methyl­formamide (DMF) as solvents. The mol­ecule is non-planar, with a C(ar­yl)—CH(2)—NH—C(ar­yl) torsion angle of −66.3 (3)°. In the crystal, O—H⋯O...

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Autores principales: Faizi, Md. Serajul Haque, Kamaal, Saima, Ali, Arif, Ahmad, Musheer, Golenya, Irina A.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2019
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6505596/
https://www.ncbi.nlm.nih.gov/pubmed/31110804
http://dx.doi.org/10.1107/S2056989019005103
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author Faizi, Md. Serajul Haque
Kamaal, Saima
Ali, Arif
Ahmad, Musheer
Golenya, Irina A.
author_facet Faizi, Md. Serajul Haque
Kamaal, Saima
Ali, Arif
Ahmad, Musheer
Golenya, Irina A.
author_sort Faizi, Md. Serajul Haque
collection PubMed
description The title compound, C(15)H(15)NO(4)·C(3)H(7)NO·H(2)O, a secondary amine mol­ecule, is accompanied by one equivalent of water and one equivalent of di­methyl­formamide (DMF) as solvents. The mol­ecule is non-planar, with a C(ar­yl)—CH(2)—NH—C(ar­yl) torsion angle of −66.3 (3)°. In the crystal, O—H⋯O and N—H⋯O hydrogen-bonding inter­actions between the amine mol­ecules and the two types of solvent mol­ecule result in the formation of a layered structure extending parallel to (010).
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spelling pubmed-65055962019-05-20 Crystal structure of 4-(2-hy­droxy-3-meth­oxy­benzyl­amino)­benzoic acid di­methyl­formamide monosolvate monohydrate Faizi, Md. Serajul Haque Kamaal, Saima Ali, Arif Ahmad, Musheer Golenya, Irina A. Acta Crystallogr E Crystallogr Commun Research Communications The title compound, C(15)H(15)NO(4)·C(3)H(7)NO·H(2)O, a secondary amine mol­ecule, is accompanied by one equivalent of water and one equivalent of di­methyl­formamide (DMF) as solvents. The mol­ecule is non-planar, with a C(ar­yl)—CH(2)—NH—C(ar­yl) torsion angle of −66.3 (3)°. In the crystal, O—H⋯O and N—H⋯O hydrogen-bonding inter­actions between the amine mol­ecules and the two types of solvent mol­ecule result in the formation of a layered structure extending parallel to (010). International Union of Crystallography 2019-04-18 /pmc/articles/PMC6505596/ /pubmed/31110804 http://dx.doi.org/10.1107/S2056989019005103 Text en © Faizi et al. 2019 http://creativecommons.org/licenses/by/4.0/ This is an open-access article distributed under the terms of the Creative Commons Attribution (CC-BY) Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.http://creativecommons.org/licenses/by/4.0/
spellingShingle Research Communications
Faizi, Md. Serajul Haque
Kamaal, Saima
Ali, Arif
Ahmad, Musheer
Golenya, Irina A.
Crystal structure of 4-(2-hy­droxy-3-meth­oxy­benzyl­amino)­benzoic acid di­methyl­formamide monosolvate monohydrate
title Crystal structure of 4-(2-hy­droxy-3-meth­oxy­benzyl­amino)­benzoic acid di­methyl­formamide monosolvate monohydrate
title_full Crystal structure of 4-(2-hy­droxy-3-meth­oxy­benzyl­amino)­benzoic acid di­methyl­formamide monosolvate monohydrate
title_fullStr Crystal structure of 4-(2-hy­droxy-3-meth­oxy­benzyl­amino)­benzoic acid di­methyl­formamide monosolvate monohydrate
title_full_unstemmed Crystal structure of 4-(2-hy­droxy-3-meth­oxy­benzyl­amino)­benzoic acid di­methyl­formamide monosolvate monohydrate
title_short Crystal structure of 4-(2-hy­droxy-3-meth­oxy­benzyl­amino)­benzoic acid di­methyl­formamide monosolvate monohydrate
title_sort crystal structure of 4-(2-hy­droxy-3-meth­oxy­benzyl­amino)­benzoic acid di­methyl­formamide monosolvate monohydrate
topic Research Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6505596/
https://www.ncbi.nlm.nih.gov/pubmed/31110804
http://dx.doi.org/10.1107/S2056989019005103
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