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Texture and Microstructural Features at Different Length Scales in Inconel 718 Produced by Selective Laser Melting

Nickel-based Inconel 718 is a very good candidate for selective laser melting (SLM). During the SLM process, Inconel 718 develops a complex and heterogeneous microstructure. A deep understanding of the microstructural features of the as-built SLM material is essential for the design of a proper post...

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Autores principales: Calandri, Michele, Yin, Shuo, Aldwell, Barry, Calignano, Flaviana, Lupoi, Rocco, Ugues, Daniele
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6514953/
https://www.ncbi.nlm.nih.gov/pubmed/31010189
http://dx.doi.org/10.3390/ma12081293
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author Calandri, Michele
Yin, Shuo
Aldwell, Barry
Calignano, Flaviana
Lupoi, Rocco
Ugues, Daniele
author_facet Calandri, Michele
Yin, Shuo
Aldwell, Barry
Calignano, Flaviana
Lupoi, Rocco
Ugues, Daniele
author_sort Calandri, Michele
collection PubMed
description Nickel-based Inconel 718 is a very good candidate for selective laser melting (SLM). During the SLM process, Inconel 718 develops a complex and heterogeneous microstructure. A deep understanding of the microstructural features of the as-built SLM material is essential for the design of a proper post-process heat treatment. In this study, the microstructure of as-built SLM Inconel 718 was investigated at different length scales using optical microscopy (OM), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). Electron backscatter diffraction (EBSD) was also used to analyze the grain morphology and crystallographic texture. Grains elongated in the build direction and crossing several deposited layers were observed. The grains are not constrained by the laser tracks or by the melt pools, which indicates epitaxial growth controls the solidification. Each grain is composed of fine columnar dendrites that develop along one of their <100> axes oriented in the direction of the local thermal gradient. Consequently, prominent <100> crystallographic texture was observed and the dendrites tend to grow to the build direction or with occasional change of 90° at the edge of the melt pools. At the dendrite length scale, the microsegregation of the alloying elements, interdendritic precipitates, and dislocations was also detected.
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spelling pubmed-65149532019-05-31 Texture and Microstructural Features at Different Length Scales in Inconel 718 Produced by Selective Laser Melting Calandri, Michele Yin, Shuo Aldwell, Barry Calignano, Flaviana Lupoi, Rocco Ugues, Daniele Materials (Basel) Article Nickel-based Inconel 718 is a very good candidate for selective laser melting (SLM). During the SLM process, Inconel 718 develops a complex and heterogeneous microstructure. A deep understanding of the microstructural features of the as-built SLM material is essential for the design of a proper post-process heat treatment. In this study, the microstructure of as-built SLM Inconel 718 was investigated at different length scales using optical microscopy (OM), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). Electron backscatter diffraction (EBSD) was also used to analyze the grain morphology and crystallographic texture. Grains elongated in the build direction and crossing several deposited layers were observed. The grains are not constrained by the laser tracks or by the melt pools, which indicates epitaxial growth controls the solidification. Each grain is composed of fine columnar dendrites that develop along one of their <100> axes oriented in the direction of the local thermal gradient. Consequently, prominent <100> crystallographic texture was observed and the dendrites tend to grow to the build direction or with occasional change of 90° at the edge of the melt pools. At the dendrite length scale, the microsegregation of the alloying elements, interdendritic precipitates, and dislocations was also detected. MDPI 2019-04-19 /pmc/articles/PMC6514953/ /pubmed/31010189 http://dx.doi.org/10.3390/ma12081293 Text en © 2019 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Calandri, Michele
Yin, Shuo
Aldwell, Barry
Calignano, Flaviana
Lupoi, Rocco
Ugues, Daniele
Texture and Microstructural Features at Different Length Scales in Inconel 718 Produced by Selective Laser Melting
title Texture and Microstructural Features at Different Length Scales in Inconel 718 Produced by Selective Laser Melting
title_full Texture and Microstructural Features at Different Length Scales in Inconel 718 Produced by Selective Laser Melting
title_fullStr Texture and Microstructural Features at Different Length Scales in Inconel 718 Produced by Selective Laser Melting
title_full_unstemmed Texture and Microstructural Features at Different Length Scales in Inconel 718 Produced by Selective Laser Melting
title_short Texture and Microstructural Features at Different Length Scales in Inconel 718 Produced by Selective Laser Melting
title_sort texture and microstructural features at different length scales in inconel 718 produced by selective laser melting
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6514953/
https://www.ncbi.nlm.nih.gov/pubmed/31010189
http://dx.doi.org/10.3390/ma12081293
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