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Micro Milled Microfluidic Photoionization Detector for Volatile Organic Compounds

Government regulations and environmental conditions are pushing the development of improved miniaturized gas analyzers for volatile organic compounds. One of the many detectors used for gas analysis is the photoionization detector (PID). This paper presents the design and characterization of a micro...

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Detalles Bibliográficos
Autores principales: Rezende, Gustavo C., Le Calvé, Stéphane, Brandner, Jürgen J., Newport, David
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6523568/
https://www.ncbi.nlm.nih.gov/pubmed/30934994
http://dx.doi.org/10.3390/mi10040228
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author Rezende, Gustavo C.
Le Calvé, Stéphane
Brandner, Jürgen J.
Newport, David
author_facet Rezende, Gustavo C.
Le Calvé, Stéphane
Brandner, Jürgen J.
Newport, David
author_sort Rezende, Gustavo C.
collection PubMed
description Government regulations and environmental conditions are pushing the development of improved miniaturized gas analyzers for volatile organic compounds. One of the many detectors used for gas analysis is the photoionization detector (PID). This paper presents the design and characterization of a microfluidic photoionization detector (or µPID) fabricated using micro milling and electrical discharge machining techniques. This device has no glue and facilitates easy replacement of components. Two materials and fabrication techniques are proposed to produce a layer on the electrodes to protect from ultraviolet (UV) light and possible signal noise generation. Three different microchannels are tested experimentally and their results are compared. The channel with highest electrode area (31.17 mm²) and higher volume (6.47 µL) produces the highest raw signal and the corresponding estimated detection limit is 0.6 ppm for toluene without any amplification unit.
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spelling pubmed-65235682019-06-03 Micro Milled Microfluidic Photoionization Detector for Volatile Organic Compounds Rezende, Gustavo C. Le Calvé, Stéphane Brandner, Jürgen J. Newport, David Micromachines (Basel) Article Government regulations and environmental conditions are pushing the development of improved miniaturized gas analyzers for volatile organic compounds. One of the many detectors used for gas analysis is the photoionization detector (PID). This paper presents the design and characterization of a microfluidic photoionization detector (or µPID) fabricated using micro milling and electrical discharge machining techniques. This device has no glue and facilitates easy replacement of components. Two materials and fabrication techniques are proposed to produce a layer on the electrodes to protect from ultraviolet (UV) light and possible signal noise generation. Three different microchannels are tested experimentally and their results are compared. The channel with highest electrode area (31.17 mm²) and higher volume (6.47 µL) produces the highest raw signal and the corresponding estimated detection limit is 0.6 ppm for toluene without any amplification unit. MDPI 2019-03-30 /pmc/articles/PMC6523568/ /pubmed/30934994 http://dx.doi.org/10.3390/mi10040228 Text en © 2019 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Rezende, Gustavo C.
Le Calvé, Stéphane
Brandner, Jürgen J.
Newport, David
Micro Milled Microfluidic Photoionization Detector for Volatile Organic Compounds
title Micro Milled Microfluidic Photoionization Detector for Volatile Organic Compounds
title_full Micro Milled Microfluidic Photoionization Detector for Volatile Organic Compounds
title_fullStr Micro Milled Microfluidic Photoionization Detector for Volatile Organic Compounds
title_full_unstemmed Micro Milled Microfluidic Photoionization Detector for Volatile Organic Compounds
title_short Micro Milled Microfluidic Photoionization Detector for Volatile Organic Compounds
title_sort micro milled microfluidic photoionization detector for volatile organic compounds
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6523568/
https://www.ncbi.nlm.nih.gov/pubmed/30934994
http://dx.doi.org/10.3390/mi10040228
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