Cargando…
Atomic resolution electron microscopy in a magnetic field free environment
Atomic-resolution electron microscopes utilize high-power magnetic lenses to produce magnified images of the atomic details of matter. Doing so involves placing samples inside the magnetic objective lens, where magnetic fields of up to a few tesla are always exerted. This can largely alter, or even...
Autores principales: | , , , , , , , , , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Nature Publishing Group UK
2019
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6534592/ https://www.ncbi.nlm.nih.gov/pubmed/31127111 http://dx.doi.org/10.1038/s41467-019-10281-2 |
_version_ | 1783421443345743872 |
---|---|
author | Shibata, N. Kohno, Y. Nakamura, A. Morishita, S. Seki, T. Kumamoto, A. Sawada, H. Matsumoto, T. Findlay, S. D. Ikuhara, Y. |
author_facet | Shibata, N. Kohno, Y. Nakamura, A. Morishita, S. Seki, T. Kumamoto, A. Sawada, H. Matsumoto, T. Findlay, S. D. Ikuhara, Y. |
author_sort | Shibata, N. |
collection | PubMed |
description | Atomic-resolution electron microscopes utilize high-power magnetic lenses to produce magnified images of the atomic details of matter. Doing so involves placing samples inside the magnetic objective lens, where magnetic fields of up to a few tesla are always exerted. This can largely alter, or even destroy, the magnetic and physical structures of interest. Here, we describe a newly developed magnetic objective lens system that realizes a magnetic field free environment at the sample position. Combined with a higher-order aberration corrector, we achieve direct, atom-resolved imaging with sub-Å spatial resolution with a residual magnetic field of less than 0.2 mT at the sample position. This capability enables direct atom-resolved imaging of magnetic materials such as silicon steels. Removing the need to subject samples to high magnetic field environments enables a new stage in atomic resolution electron microscopy that realizes direct, atomic-level observation of samples without unwanted high magnetic field effects. |
format | Online Article Text |
id | pubmed-6534592 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2019 |
publisher | Nature Publishing Group UK |
record_format | MEDLINE/PubMed |
spelling | pubmed-65345922019-05-28 Atomic resolution electron microscopy in a magnetic field free environment Shibata, N. Kohno, Y. Nakamura, A. Morishita, S. Seki, T. Kumamoto, A. Sawada, H. Matsumoto, T. Findlay, S. D. Ikuhara, Y. Nat Commun Article Atomic-resolution electron microscopes utilize high-power magnetic lenses to produce magnified images of the atomic details of matter. Doing so involves placing samples inside the magnetic objective lens, where magnetic fields of up to a few tesla are always exerted. This can largely alter, or even destroy, the magnetic and physical structures of interest. Here, we describe a newly developed magnetic objective lens system that realizes a magnetic field free environment at the sample position. Combined with a higher-order aberration corrector, we achieve direct, atom-resolved imaging with sub-Å spatial resolution with a residual magnetic field of less than 0.2 mT at the sample position. This capability enables direct atom-resolved imaging of magnetic materials such as silicon steels. Removing the need to subject samples to high magnetic field environments enables a new stage in atomic resolution electron microscopy that realizes direct, atomic-level observation of samples without unwanted high magnetic field effects. Nature Publishing Group UK 2019-05-24 /pmc/articles/PMC6534592/ /pubmed/31127111 http://dx.doi.org/10.1038/s41467-019-10281-2 Text en © The Author(s) 2019 Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/. |
spellingShingle | Article Shibata, N. Kohno, Y. Nakamura, A. Morishita, S. Seki, T. Kumamoto, A. Sawada, H. Matsumoto, T. Findlay, S. D. Ikuhara, Y. Atomic resolution electron microscopy in a magnetic field free environment |
title | Atomic resolution electron microscopy in a magnetic field free environment |
title_full | Atomic resolution electron microscopy in a magnetic field free environment |
title_fullStr | Atomic resolution electron microscopy in a magnetic field free environment |
title_full_unstemmed | Atomic resolution electron microscopy in a magnetic field free environment |
title_short | Atomic resolution electron microscopy in a magnetic field free environment |
title_sort | atomic resolution electron microscopy in a magnetic field free environment |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6534592/ https://www.ncbi.nlm.nih.gov/pubmed/31127111 http://dx.doi.org/10.1038/s41467-019-10281-2 |
work_keys_str_mv | AT shibatan atomicresolutionelectronmicroscopyinamagneticfieldfreeenvironment AT kohnoy atomicresolutionelectronmicroscopyinamagneticfieldfreeenvironment AT nakamuraa atomicresolutionelectronmicroscopyinamagneticfieldfreeenvironment AT morishitas atomicresolutionelectronmicroscopyinamagneticfieldfreeenvironment AT sekit atomicresolutionelectronmicroscopyinamagneticfieldfreeenvironment AT kumamotoa atomicresolutionelectronmicroscopyinamagneticfieldfreeenvironment AT sawadah atomicresolutionelectronmicroscopyinamagneticfieldfreeenvironment AT matsumotot atomicresolutionelectronmicroscopyinamagneticfieldfreeenvironment AT findlaysd atomicresolutionelectronmicroscopyinamagneticfieldfreeenvironment AT ikuharay atomicresolutionelectronmicroscopyinamagneticfieldfreeenvironment |