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Atomic resolution electron microscopy in a magnetic field free environment

Atomic-resolution electron microscopes utilize high-power magnetic lenses to produce magnified images of the atomic details of matter. Doing so involves placing samples inside the magnetic objective lens, where magnetic fields of up to a few tesla are always exerted. This can largely alter, or even...

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Autores principales: Shibata, N., Kohno, Y., Nakamura, A., Morishita, S., Seki, T., Kumamoto, A., Sawada, H., Matsumoto, T., Findlay, S. D., Ikuhara, Y.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6534592/
https://www.ncbi.nlm.nih.gov/pubmed/31127111
http://dx.doi.org/10.1038/s41467-019-10281-2
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author Shibata, N.
Kohno, Y.
Nakamura, A.
Morishita, S.
Seki, T.
Kumamoto, A.
Sawada, H.
Matsumoto, T.
Findlay, S. D.
Ikuhara, Y.
author_facet Shibata, N.
Kohno, Y.
Nakamura, A.
Morishita, S.
Seki, T.
Kumamoto, A.
Sawada, H.
Matsumoto, T.
Findlay, S. D.
Ikuhara, Y.
author_sort Shibata, N.
collection PubMed
description Atomic-resolution electron microscopes utilize high-power magnetic lenses to produce magnified images of the atomic details of matter. Doing so involves placing samples inside the magnetic objective lens, where magnetic fields of up to a few tesla are always exerted. This can largely alter, or even destroy, the magnetic and physical structures of interest. Here, we describe a newly developed magnetic objective lens system that realizes a magnetic field free environment at the sample position. Combined with a higher-order aberration corrector, we achieve direct, atom-resolved imaging with sub-Å spatial resolution with a residual magnetic field of less than 0.2 mT at the sample position. This capability enables direct atom-resolved imaging of magnetic materials such as silicon steels. Removing the need to subject samples to high magnetic field environments enables a new stage in atomic resolution electron microscopy that realizes direct, atomic-level observation of samples without unwanted high magnetic field effects.
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spelling pubmed-65345922019-05-28 Atomic resolution electron microscopy in a magnetic field free environment Shibata, N. Kohno, Y. Nakamura, A. Morishita, S. Seki, T. Kumamoto, A. Sawada, H. Matsumoto, T. Findlay, S. D. Ikuhara, Y. Nat Commun Article Atomic-resolution electron microscopes utilize high-power magnetic lenses to produce magnified images of the atomic details of matter. Doing so involves placing samples inside the magnetic objective lens, where magnetic fields of up to a few tesla are always exerted. This can largely alter, or even destroy, the magnetic and physical structures of interest. Here, we describe a newly developed magnetic objective lens system that realizes a magnetic field free environment at the sample position. Combined with a higher-order aberration corrector, we achieve direct, atom-resolved imaging with sub-Å spatial resolution with a residual magnetic field of less than 0.2 mT at the sample position. This capability enables direct atom-resolved imaging of magnetic materials such as silicon steels. Removing the need to subject samples to high magnetic field environments enables a new stage in atomic resolution electron microscopy that realizes direct, atomic-level observation of samples without unwanted high magnetic field effects. Nature Publishing Group UK 2019-05-24 /pmc/articles/PMC6534592/ /pubmed/31127111 http://dx.doi.org/10.1038/s41467-019-10281-2 Text en © The Author(s) 2019 Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.
spellingShingle Article
Shibata, N.
Kohno, Y.
Nakamura, A.
Morishita, S.
Seki, T.
Kumamoto, A.
Sawada, H.
Matsumoto, T.
Findlay, S. D.
Ikuhara, Y.
Atomic resolution electron microscopy in a magnetic field free environment
title Atomic resolution electron microscopy in a magnetic field free environment
title_full Atomic resolution electron microscopy in a magnetic field free environment
title_fullStr Atomic resolution electron microscopy in a magnetic field free environment
title_full_unstemmed Atomic resolution electron microscopy in a magnetic field free environment
title_short Atomic resolution electron microscopy in a magnetic field free environment
title_sort atomic resolution electron microscopy in a magnetic field free environment
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6534592/
https://www.ncbi.nlm.nih.gov/pubmed/31127111
http://dx.doi.org/10.1038/s41467-019-10281-2
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