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Data Correction of Intensity Modulated Small Angle Scattering

To investigate long length scale structures using neutron scattering, real space techniques have shown certain advantages over the conventional methods working in reciprocal space. As one of the real space measurement techniques, spin echo modulated small angle neutron scattering (SEMSANS) has attra...

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Autores principales: Li, Fankang, Parnell, Steven R., Dalgliesh, Robert, Washington, Adam, Plomp, Jeroen, Pynn, Roger
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Nature Publishing Group UK 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6561909/
https://www.ncbi.nlm.nih.gov/pubmed/31189935
http://dx.doi.org/10.1038/s41598-019-44493-9
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author Li, Fankang
Parnell, Steven R.
Dalgliesh, Robert
Washington, Adam
Plomp, Jeroen
Pynn, Roger
author_facet Li, Fankang
Parnell, Steven R.
Dalgliesh, Robert
Washington, Adam
Plomp, Jeroen
Pynn, Roger
author_sort Li, Fankang
collection PubMed
description To investigate long length scale structures using neutron scattering, real space techniques have shown certain advantages over the conventional methods working in reciprocal space. As one of the real space measurement techniques, spin echo modulated small angle neutron scattering (SEMSANS) has attracted attention, due to its relaxed constraints on sample environment and the possibility to combine SEMSANS and a conventional small angle neutron scattering instrument. In this report, we present the first implementation of SEMSANS at a pulsed neutron source and discuss important corrections to the data due to the sample absorption. These corrections allow measurements made with different neutron wavelengths and SEMSANS configurations to be overlaid and give confidence that the measurements provide an accurate representation of the density correlations in the sample.
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spelling pubmed-65619092019-06-19 Data Correction of Intensity Modulated Small Angle Scattering Li, Fankang Parnell, Steven R. Dalgliesh, Robert Washington, Adam Plomp, Jeroen Pynn, Roger Sci Rep Article To investigate long length scale structures using neutron scattering, real space techniques have shown certain advantages over the conventional methods working in reciprocal space. As one of the real space measurement techniques, spin echo modulated small angle neutron scattering (SEMSANS) has attracted attention, due to its relaxed constraints on sample environment and the possibility to combine SEMSANS and a conventional small angle neutron scattering instrument. In this report, we present the first implementation of SEMSANS at a pulsed neutron source and discuss important corrections to the data due to the sample absorption. These corrections allow measurements made with different neutron wavelengths and SEMSANS configurations to be overlaid and give confidence that the measurements provide an accurate representation of the density correlations in the sample. Nature Publishing Group UK 2019-06-12 /pmc/articles/PMC6561909/ /pubmed/31189935 http://dx.doi.org/10.1038/s41598-019-44493-9 Text en © The Author(s) 2019 Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/.
spellingShingle Article
Li, Fankang
Parnell, Steven R.
Dalgliesh, Robert
Washington, Adam
Plomp, Jeroen
Pynn, Roger
Data Correction of Intensity Modulated Small Angle Scattering
title Data Correction of Intensity Modulated Small Angle Scattering
title_full Data Correction of Intensity Modulated Small Angle Scattering
title_fullStr Data Correction of Intensity Modulated Small Angle Scattering
title_full_unstemmed Data Correction of Intensity Modulated Small Angle Scattering
title_short Data Correction of Intensity Modulated Small Angle Scattering
title_sort data correction of intensity modulated small angle scattering
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6561909/
https://www.ncbi.nlm.nih.gov/pubmed/31189935
http://dx.doi.org/10.1038/s41598-019-44493-9
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