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Direct Measurement of the In-Plane Thermal Diffusivity of Semitransparent Thin Films by Lock-In Thermography: An Extension of the Slopes Method
[Image: see text] We present an extension of the well-known slopes method for characterization of the in-plane thermal diffusivity of semitransparent polymer films. We introduce a theoretical model which considers heat losses due to convection and radiation mechanisms, as well as semitransparency of...
Autores principales: | , , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
American
Chemical
Society
2019
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Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6613730/ https://www.ncbi.nlm.nih.gov/pubmed/31148451 http://dx.doi.org/10.1021/acs.analchem.9b01583 |
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author | Philipp, Alexandra Pech-May, Nelson W. Kopera, Bernd A. F. Lechner, Anna M. Rosenfeldt, Sabine Retsch, Markus |
author_facet | Philipp, Alexandra Pech-May, Nelson W. Kopera, Bernd A. F. Lechner, Anna M. Rosenfeldt, Sabine Retsch, Markus |
author_sort | Philipp, Alexandra |
collection | PubMed |
description | [Image: see text] We present an extension of the well-known slopes method for characterization of the in-plane thermal diffusivity of semitransparent polymer films. We introduce a theoretical model which considers heat losses due to convection and radiation mechanisms, as well as semitransparency of the material to the exciting laser heat source (visible range) and multiple reflections at the film surfaces. Most importantly, a potential semitransparency of the material in the IR detection range is also considered. We prove by numerical simulations and by an asymptotic expansion of the surface temperature that the slopes method is also valid for any semitransparent film in the thermally thin regime. Measurements of the in-plane thermal diffusivity performed on semitransparent polymer films covering a wide range of absorption coefficients (to the exciting wavelength and in the IR detection range of our IR camera) validate our theoretical findings. |
format | Online Article Text |
id | pubmed-6613730 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2019 |
publisher | American
Chemical
Society |
record_format | MEDLINE/PubMed |
spelling | pubmed-66137302019-07-09 Direct Measurement of the In-Plane Thermal Diffusivity of Semitransparent Thin Films by Lock-In Thermography: An Extension of the Slopes Method Philipp, Alexandra Pech-May, Nelson W. Kopera, Bernd A. F. Lechner, Anna M. Rosenfeldt, Sabine Retsch, Markus Anal Chem [Image: see text] We present an extension of the well-known slopes method for characterization of the in-plane thermal diffusivity of semitransparent polymer films. We introduce a theoretical model which considers heat losses due to convection and radiation mechanisms, as well as semitransparency of the material to the exciting laser heat source (visible range) and multiple reflections at the film surfaces. Most importantly, a potential semitransparency of the material in the IR detection range is also considered. We prove by numerical simulations and by an asymptotic expansion of the surface temperature that the slopes method is also valid for any semitransparent film in the thermally thin regime. Measurements of the in-plane thermal diffusivity performed on semitransparent polymer films covering a wide range of absorption coefficients (to the exciting wavelength and in the IR detection range of our IR camera) validate our theoretical findings. American Chemical Society 2019-05-31 2019-07-02 /pmc/articles/PMC6613730/ /pubmed/31148451 http://dx.doi.org/10.1021/acs.analchem.9b01583 Text en Copyright © 2019 American Chemical Society This is an open access article published under a Creative Commons Attribution (CC-BY) License (http://pubs.acs.org/page/policy/authorchoice_ccby_termsofuse.html) , which permits unrestricted use, distribution and reproduction in any medium, provided the author and source are cited. |
spellingShingle | Philipp, Alexandra Pech-May, Nelson W. Kopera, Bernd A. F. Lechner, Anna M. Rosenfeldt, Sabine Retsch, Markus Direct Measurement of the In-Plane Thermal Diffusivity of Semitransparent Thin Films by Lock-In Thermography: An Extension of the Slopes Method |
title | Direct Measurement of the In-Plane Thermal Diffusivity
of Semitransparent Thin Films by Lock-In Thermography: An Extension
of the Slopes Method |
title_full | Direct Measurement of the In-Plane Thermal Diffusivity
of Semitransparent Thin Films by Lock-In Thermography: An Extension
of the Slopes Method |
title_fullStr | Direct Measurement of the In-Plane Thermal Diffusivity
of Semitransparent Thin Films by Lock-In Thermography: An Extension
of the Slopes Method |
title_full_unstemmed | Direct Measurement of the In-Plane Thermal Diffusivity
of Semitransparent Thin Films by Lock-In Thermography: An Extension
of the Slopes Method |
title_short | Direct Measurement of the In-Plane Thermal Diffusivity
of Semitransparent Thin Films by Lock-In Thermography: An Extension
of the Slopes Method |
title_sort | direct measurement of the in-plane thermal diffusivity
of semitransparent thin films by lock-in thermography: an extension
of the slopes method |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6613730/ https://www.ncbi.nlm.nih.gov/pubmed/31148451 http://dx.doi.org/10.1021/acs.analchem.9b01583 |
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