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3D Printed UV–Visible Cuvette Adapter for Low-Cost and Versatile Spectroscopic Experiments

[Image: see text] Ultraviolet–visible (UV–vis) spectroscopy represents one of the most popular analytical techniques in chemical research labs. A variety of vendors provide instruments that are suited for the analysis of liquid samples at moderate concentrations. However, to accommodate more special...

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Autores principales: Whitehead, Heather D., Waldman, Julia V., Wirth, Denise M., LeBlanc, Gabriel
Formato: Online Artículo Texto
Lenguaje:English
Publicado: American Chemical Society 2017
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6644542/
https://www.ncbi.nlm.nih.gov/pubmed/31457858
http://dx.doi.org/10.1021/acsomega.7b01310
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author Whitehead, Heather D.
Waldman, Julia V.
Wirth, Denise M.
LeBlanc, Gabriel
author_facet Whitehead, Heather D.
Waldman, Julia V.
Wirth, Denise M.
LeBlanc, Gabriel
author_sort Whitehead, Heather D.
collection PubMed
description [Image: see text] Ultraviolet–visible (UV–vis) spectroscopy represents one of the most popular analytical techniques in chemical research labs. A variety of vendors provide instruments that are suited for the analysis of liquid samples at moderate concentrations. However, to accommodate more specialized experiments, expensive accessories are required and often do not fit the specific needs of experimental scientists. In this work, we present a generalized adapter that can be 3D printed and used with existing spectrometers to enable a wide array of experiments to be performed. In the case of liquid samples, we provide a method for dramatically reducing the price of a quartz cuvette with minimal impact on performance. Through simple modification of the design, cuvettes with various path lengths can be prepared. Additionally, we illustrate the ability to turn any sample container into a working cuvette to simplify experimental protocols, prevent contamination risks, and further reduce costs. This strategy also enables gaseous and solid samples to be evaluated easily and reproducibly. Furthermore, we demonstrate how this concept can be extended to interface additional instrumentation with a commercial UV–vis spectrometer. All of the digital designs are provided under a creative commons license to enable other researchers to modify and adapt the designs for their unique experimental requirements.
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spelling pubmed-66445422019-08-27 3D Printed UV–Visible Cuvette Adapter for Low-Cost and Versatile Spectroscopic Experiments Whitehead, Heather D. Waldman, Julia V. Wirth, Denise M. LeBlanc, Gabriel ACS Omega [Image: see text] Ultraviolet–visible (UV–vis) spectroscopy represents one of the most popular analytical techniques in chemical research labs. A variety of vendors provide instruments that are suited for the analysis of liquid samples at moderate concentrations. However, to accommodate more specialized experiments, expensive accessories are required and often do not fit the specific needs of experimental scientists. In this work, we present a generalized adapter that can be 3D printed and used with existing spectrometers to enable a wide array of experiments to be performed. In the case of liquid samples, we provide a method for dramatically reducing the price of a quartz cuvette with minimal impact on performance. Through simple modification of the design, cuvettes with various path lengths can be prepared. Additionally, we illustrate the ability to turn any sample container into a working cuvette to simplify experimental protocols, prevent contamination risks, and further reduce costs. This strategy also enables gaseous and solid samples to be evaluated easily and reproducibly. Furthermore, we demonstrate how this concept can be extended to interface additional instrumentation with a commercial UV–vis spectrometer. All of the digital designs are provided under a creative commons license to enable other researchers to modify and adapt the designs for their unique experimental requirements. American Chemical Society 2017-09-25 /pmc/articles/PMC6644542/ /pubmed/31457858 http://dx.doi.org/10.1021/acsomega.7b01310 Text en Copyright © 2017 American Chemical Society This is an open access article published under a Creative Commons Attribution (CC-BY) License (http://pubs.acs.org/page/policy/authorchoice_ccby_termsofuse.html) , which permits unrestricted use, distribution and reproduction in any medium, provided the author and source are cited.
spellingShingle Whitehead, Heather D.
Waldman, Julia V.
Wirth, Denise M.
LeBlanc, Gabriel
3D Printed UV–Visible Cuvette Adapter for Low-Cost and Versatile Spectroscopic Experiments
title 3D Printed UV–Visible Cuvette Adapter for Low-Cost and Versatile Spectroscopic Experiments
title_full 3D Printed UV–Visible Cuvette Adapter for Low-Cost and Versatile Spectroscopic Experiments
title_fullStr 3D Printed UV–Visible Cuvette Adapter for Low-Cost and Versatile Spectroscopic Experiments
title_full_unstemmed 3D Printed UV–Visible Cuvette Adapter for Low-Cost and Versatile Spectroscopic Experiments
title_short 3D Printed UV–Visible Cuvette Adapter for Low-Cost and Versatile Spectroscopic Experiments
title_sort 3d printed uv–visible cuvette adapter for low-cost and versatile spectroscopic experiments
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6644542/
https://www.ncbi.nlm.nih.gov/pubmed/31457858
http://dx.doi.org/10.1021/acsomega.7b01310
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