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Co-aminobenzamid@Al-SBA-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1H)-ones
The novel hybrid Co-aminobenzamid@Al-SBA-15 was synthesized as a modified mesoporous catalyst. To achieve this aim, the obtained materials were investigated by various techniques including Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), N(2) adsorption–desorption, field emi...
Autores principales: | , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
Springer International Publishing
2019
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6659566/ https://www.ncbi.nlm.nih.gov/pubmed/31355367 http://dx.doi.org/10.1186/s13065-019-0517-7 |
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author | Safaei-Ghomi, Javad Teymuri, Raheleh Bakhtiari, Atefeh |
author_facet | Safaei-Ghomi, Javad Teymuri, Raheleh Bakhtiari, Atefeh |
author_sort | Safaei-Ghomi, Javad |
collection | PubMed |
description | The novel hybrid Co-aminobenzamid@Al-SBA-15 was synthesized as a modified mesoporous catalyst. To achieve this aim, the obtained materials were investigated by various techniques including Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), N(2) adsorption–desorption, field emission scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM) to examine the functional groups, crystallinity, surface area, morphology, particle size distribution and amounts of functional groups, respectively. Co-aminobenzamid@Al-SBA-15 exhibits excellent catalytic activity for the synthesis of 2,3-dihydroquinazolin-4(1H)-ones under mild reaction conditions. The heterogeneous catalyst showed good recyclability and can be reused for ten consecutive cycles without significant loss of its catalytic activity. [Image: see text] ELECTRONIC SUPPLEMENTARY MATERIAL: The online version of this article (10.1186/s13065-019-0517-7) contains supplementary material, which is available to authorized users. |
format | Online Article Text |
id | pubmed-6659566 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2019 |
publisher | Springer International Publishing |
record_format | MEDLINE/PubMed |
spelling | pubmed-66595662019-07-26 Co-aminobenzamid@Al-SBA-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1H)-ones Safaei-Ghomi, Javad Teymuri, Raheleh Bakhtiari, Atefeh BMC Chem Research Article The novel hybrid Co-aminobenzamid@Al-SBA-15 was synthesized as a modified mesoporous catalyst. To achieve this aim, the obtained materials were investigated by various techniques including Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), N(2) adsorption–desorption, field emission scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM) to examine the functional groups, crystallinity, surface area, morphology, particle size distribution and amounts of functional groups, respectively. Co-aminobenzamid@Al-SBA-15 exhibits excellent catalytic activity for the synthesis of 2,3-dihydroquinazolin-4(1H)-ones under mild reaction conditions. The heterogeneous catalyst showed good recyclability and can be reused for ten consecutive cycles without significant loss of its catalytic activity. [Image: see text] ELECTRONIC SUPPLEMENTARY MATERIAL: The online version of this article (10.1186/s13065-019-0517-7) contains supplementary material, which is available to authorized users. Springer International Publishing 2019-02-28 /pmc/articles/PMC6659566/ /pubmed/31355367 http://dx.doi.org/10.1186/s13065-019-0517-7 Text en © The Author(s) 2019 Open AccessThis article is distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The Creative Commons Public Domain Dedication waiver (http://creativecommons.org/publicdomain/zero/1.0/) applies to the data made available in this article, unless otherwise stated. |
spellingShingle | Research Article Safaei-Ghomi, Javad Teymuri, Raheleh Bakhtiari, Atefeh Co-aminobenzamid@Al-SBA-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1H)-ones |
title | Co-aminobenzamid@Al-SBA-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1H)-ones |
title_full | Co-aminobenzamid@Al-SBA-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1H)-ones |
title_fullStr | Co-aminobenzamid@Al-SBA-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1H)-ones |
title_full_unstemmed | Co-aminobenzamid@Al-SBA-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1H)-ones |
title_short | Co-aminobenzamid@Al-SBA-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1H)-ones |
title_sort | co-aminobenzamid@al-sba-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1h)-ones |
topic | Research Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6659566/ https://www.ncbi.nlm.nih.gov/pubmed/31355367 http://dx.doi.org/10.1186/s13065-019-0517-7 |
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