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Co-aminobenzamid@Al-SBA-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1H)-ones

The novel hybrid Co-aminobenzamid@Al-SBA-15 was synthesized as a modified mesoporous catalyst. To achieve this aim, the obtained materials were investigated by various techniques including Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), N(2) adsorption–desorption, field emi...

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Autores principales: Safaei-Ghomi, Javad, Teymuri, Raheleh, Bakhtiari, Atefeh
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Springer International Publishing 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6659566/
https://www.ncbi.nlm.nih.gov/pubmed/31355367
http://dx.doi.org/10.1186/s13065-019-0517-7
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author Safaei-Ghomi, Javad
Teymuri, Raheleh
Bakhtiari, Atefeh
author_facet Safaei-Ghomi, Javad
Teymuri, Raheleh
Bakhtiari, Atefeh
author_sort Safaei-Ghomi, Javad
collection PubMed
description The novel hybrid Co-aminobenzamid@Al-SBA-15 was synthesized as a modified mesoporous catalyst. To achieve this aim, the obtained materials were investigated by various techniques including Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), N(2) adsorption–desorption, field emission scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM) to examine the functional groups, crystallinity, surface area, morphology, particle size distribution and amounts of functional groups, respectively. Co-aminobenzamid@Al-SBA-15 exhibits excellent catalytic activity for the synthesis of 2,3-dihydroquinazolin-4(1H)-ones under mild reaction conditions. The heterogeneous catalyst showed good recyclability and can be reused for ten consecutive cycles without significant loss of its catalytic activity. [Image: see text] ELECTRONIC SUPPLEMENTARY MATERIAL: The online version of this article (10.1186/s13065-019-0517-7) contains supplementary material, which is available to authorized users.
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spelling pubmed-66595662019-07-26 Co-aminobenzamid@Al-SBA-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1H)-ones Safaei-Ghomi, Javad Teymuri, Raheleh Bakhtiari, Atefeh BMC Chem Research Article The novel hybrid Co-aminobenzamid@Al-SBA-15 was synthesized as a modified mesoporous catalyst. To achieve this aim, the obtained materials were investigated by various techniques including Fourier transform infrared spectroscopy (FT-IR), X-ray diffraction (XRD), N(2) adsorption–desorption, field emission scanning electron microscopy (FE-SEM) and transmission electron microscopy (TEM) to examine the functional groups, crystallinity, surface area, morphology, particle size distribution and amounts of functional groups, respectively. Co-aminobenzamid@Al-SBA-15 exhibits excellent catalytic activity for the synthesis of 2,3-dihydroquinazolin-4(1H)-ones under mild reaction conditions. The heterogeneous catalyst showed good recyclability and can be reused for ten consecutive cycles without significant loss of its catalytic activity. [Image: see text] ELECTRONIC SUPPLEMENTARY MATERIAL: The online version of this article (10.1186/s13065-019-0517-7) contains supplementary material, which is available to authorized users. Springer International Publishing 2019-02-28 /pmc/articles/PMC6659566/ /pubmed/31355367 http://dx.doi.org/10.1186/s13065-019-0517-7 Text en © The Author(s) 2019 Open AccessThis article is distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The Creative Commons Public Domain Dedication waiver (http://creativecommons.org/publicdomain/zero/1.0/) applies to the data made available in this article, unless otherwise stated.
spellingShingle Research Article
Safaei-Ghomi, Javad
Teymuri, Raheleh
Bakhtiari, Atefeh
Co-aminobenzamid@Al-SBA-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1H)-ones
title Co-aminobenzamid@Al-SBA-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1H)-ones
title_full Co-aminobenzamid@Al-SBA-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1H)-ones
title_fullStr Co-aminobenzamid@Al-SBA-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1H)-ones
title_full_unstemmed Co-aminobenzamid@Al-SBA-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1H)-ones
title_short Co-aminobenzamid@Al-SBA-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1H)-ones
title_sort co-aminobenzamid@al-sba-15: a favorable catalyst in synthesis of 2,3-dihydroquinazolin-4(1h)-ones
topic Research Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6659566/
https://www.ncbi.nlm.nih.gov/pubmed/31355367
http://dx.doi.org/10.1186/s13065-019-0517-7
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