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Crystal structures of three cyclohexane-based γ-spirolactams: determination of configurations and conformations

The title compounds, 2-azaspiro[4.5]deca-1-one, C(9)H(15)NO, (1a), cis-8-methyl-2-azaspiro[4.5]deca-1-one, C(10)H(17)NO, (1b), and trans-8-methyl-2-azaspiro[4.5]deca-1-one, C(10)H(17)NO, (1c), were synthesized from benzoic acids 2 in only 3 steps in high yields. Crystallization from n-hexane afforde...

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Detalles Bibliográficos
Autores principales:	Krueger, Tobias, Kelling, Alexandra, Linker, Torsten, Schilde, Uwe
Formato:	Online Artículo Texto
Lenguaje:	English
Publicado:	Springer International Publishing 2019
Materias:	Research Article
Acceso en línea:	https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6661822/ https://www.ncbi.nlm.nih.gov/pubmed/31384816 http://dx.doi.org/10.1186/s13065-019-0586-7

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