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High-speed crystal detection and characterization using a fast-readout detector

A novel raster-scanning method combining continuous sample translation with the fast readout of a Pilatus P6M detector has been developed on microfocus beamline I24 at Diamond Light Source. This fast grid-scan tool allows the rapid evaluation of large sample volumes without the need to increase the...

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Detalles Bibliográficos
Autores principales: Aishima, Jun, Owen, Robin L., Axford, Danny, Shepherd, Emma, Winter, Graeme, Levik, Karl, Gibbons, Paul, Ashton, Alun, Evans, Gwyndaf
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2010
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6691516/
https://www.ncbi.nlm.nih.gov/pubmed/20823554
http://dx.doi.org/10.1107/S0907444910028192
Descripción
Sumario:A novel raster-scanning method combining continuous sample translation with the fast readout of a Pilatus P6M detector has been developed on microfocus beamline I24 at Diamond Light Source. This fast grid-scan tool allows the rapid evaluation of large sample volumes without the need to increase the beam size at the sample through changes in beamline hardware. A slow version is available for slow-readout detectors. Examples of grid-scan use in centring optically invisible samples and in detecting and characterizing numerous microcrystals on a mesh-like holder illustrate the most common applications of the grid scan now in routine use on I24.