Cargando…
Solvent-Free Preparation of 1,8-Dioxo-Octahydroxanthenes Employing Iron Oxide Nanomaterials
In this study, 1,8-dioxo-octahydroxanthenes were prepared employing a simple, effective and environmentally sound approach utilizing an iron oxide nanocatalyst under solventless conditions. The proposed iron oxide nanomaterial exhibited high product yields, short reaction times and a facile work-up...
Autores principales: | , , , , , , , |
---|---|
Formato: | Online Artículo Texto |
Lenguaje: | English |
Publicado: |
MDPI
2019
|
Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6695819/ https://www.ncbi.nlm.nih.gov/pubmed/31357446 http://dx.doi.org/10.3390/ma12152386 |
_version_ | 1783444124509143040 |
---|---|
author | Rajabi, Fatemeh Abdollahi, Mohammad Diarjani, Elham Sadat Osmolowsky, Mikhail G. Osmolovskaya, Olga M. Gómez-López, Paulette Puente-Santiago, Alain R. Luque, Rafael |
author_facet | Rajabi, Fatemeh Abdollahi, Mohammad Diarjani, Elham Sadat Osmolowsky, Mikhail G. Osmolovskaya, Olga M. Gómez-López, Paulette Puente-Santiago, Alain R. Luque, Rafael |
author_sort | Rajabi, Fatemeh |
collection | PubMed |
description | In this study, 1,8-dioxo-octahydroxanthenes were prepared employing a simple, effective and environmentally sound approach utilizing an iron oxide nanocatalyst under solventless conditions. The proposed iron oxide nanomaterial exhibited high product yields, short reaction times and a facile work-up procedure. The synthesized catalyst was also found to be highly stable and reusable under the investigated conditions (up to twelve consecutive cycles) without any significant loss in its catalytic activity. |
format | Online Article Text |
id | pubmed-6695819 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2019 |
publisher | MDPI |
record_format | MEDLINE/PubMed |
spelling | pubmed-66958192019-09-05 Solvent-Free Preparation of 1,8-Dioxo-Octahydroxanthenes Employing Iron Oxide Nanomaterials Rajabi, Fatemeh Abdollahi, Mohammad Diarjani, Elham Sadat Osmolowsky, Mikhail G. Osmolovskaya, Olga M. Gómez-López, Paulette Puente-Santiago, Alain R. Luque, Rafael Materials (Basel) Article In this study, 1,8-dioxo-octahydroxanthenes were prepared employing a simple, effective and environmentally sound approach utilizing an iron oxide nanocatalyst under solventless conditions. The proposed iron oxide nanomaterial exhibited high product yields, short reaction times and a facile work-up procedure. The synthesized catalyst was also found to be highly stable and reusable under the investigated conditions (up to twelve consecutive cycles) without any significant loss in its catalytic activity. MDPI 2019-07-26 /pmc/articles/PMC6695819/ /pubmed/31357446 http://dx.doi.org/10.3390/ma12152386 Text en © 2019 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/). |
spellingShingle | Article Rajabi, Fatemeh Abdollahi, Mohammad Diarjani, Elham Sadat Osmolowsky, Mikhail G. Osmolovskaya, Olga M. Gómez-López, Paulette Puente-Santiago, Alain R. Luque, Rafael Solvent-Free Preparation of 1,8-Dioxo-Octahydroxanthenes Employing Iron Oxide Nanomaterials |
title | Solvent-Free Preparation of 1,8-Dioxo-Octahydroxanthenes Employing Iron Oxide Nanomaterials |
title_full | Solvent-Free Preparation of 1,8-Dioxo-Octahydroxanthenes Employing Iron Oxide Nanomaterials |
title_fullStr | Solvent-Free Preparation of 1,8-Dioxo-Octahydroxanthenes Employing Iron Oxide Nanomaterials |
title_full_unstemmed | Solvent-Free Preparation of 1,8-Dioxo-Octahydroxanthenes Employing Iron Oxide Nanomaterials |
title_short | Solvent-Free Preparation of 1,8-Dioxo-Octahydroxanthenes Employing Iron Oxide Nanomaterials |
title_sort | solvent-free preparation of 1,8-dioxo-octahydroxanthenes employing iron oxide nanomaterials |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6695819/ https://www.ncbi.nlm.nih.gov/pubmed/31357446 http://dx.doi.org/10.3390/ma12152386 |
work_keys_str_mv | AT rajabifatemeh solventfreepreparationof18dioxooctahydroxanthenesemployingironoxidenanomaterials AT abdollahimohammad solventfreepreparationof18dioxooctahydroxanthenesemployingironoxidenanomaterials AT diarjanielhamsadat solventfreepreparationof18dioxooctahydroxanthenesemployingironoxidenanomaterials AT osmolowskymikhailg solventfreepreparationof18dioxooctahydroxanthenesemployingironoxidenanomaterials AT osmolovskayaolgam solventfreepreparationof18dioxooctahydroxanthenesemployingironoxidenanomaterials AT gomezlopezpaulette solventfreepreparationof18dioxooctahydroxanthenesemployingironoxidenanomaterials AT puentesantiagoalainr solventfreepreparationof18dioxooctahydroxanthenesemployingironoxidenanomaterials AT luquerafael solventfreepreparationof18dioxooctahydroxanthenesemployingironoxidenanomaterials |