Cargando…

Solvent-Free Preparation of 1,8-Dioxo-Octahydroxanthenes Employing Iron Oxide Nanomaterials

In this study, 1,8-dioxo-octahydroxanthenes were prepared employing a simple, effective and environmentally sound approach utilizing an iron oxide nanocatalyst under solventless conditions. The proposed iron oxide nanomaterial exhibited high product yields, short reaction times and a facile work-up...

Descripción completa

Detalles Bibliográficos
Autores principales: Rajabi, Fatemeh, Abdollahi, Mohammad, Diarjani, Elham Sadat, Osmolowsky, Mikhail G., Osmolovskaya, Olga M., Gómez-López, Paulette, Puente-Santiago, Alain R., Luque, Rafael
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6695819/
https://www.ncbi.nlm.nih.gov/pubmed/31357446
http://dx.doi.org/10.3390/ma12152386
_version_ 1783444124509143040
author Rajabi, Fatemeh
Abdollahi, Mohammad
Diarjani, Elham Sadat
Osmolowsky, Mikhail G.
Osmolovskaya, Olga M.
Gómez-López, Paulette
Puente-Santiago, Alain R.
Luque, Rafael
author_facet Rajabi, Fatemeh
Abdollahi, Mohammad
Diarjani, Elham Sadat
Osmolowsky, Mikhail G.
Osmolovskaya, Olga M.
Gómez-López, Paulette
Puente-Santiago, Alain R.
Luque, Rafael
author_sort Rajabi, Fatemeh
collection PubMed
description In this study, 1,8-dioxo-octahydroxanthenes were prepared employing a simple, effective and environmentally sound approach utilizing an iron oxide nanocatalyst under solventless conditions. The proposed iron oxide nanomaterial exhibited high product yields, short reaction times and a facile work-up procedure. The synthesized catalyst was also found to be highly stable and reusable under the investigated conditions (up to twelve consecutive cycles) without any significant loss in its catalytic activity.
format Online
Article
Text
id pubmed-6695819
institution National Center for Biotechnology Information
language English
publishDate 2019
publisher MDPI
record_format MEDLINE/PubMed
spelling pubmed-66958192019-09-05 Solvent-Free Preparation of 1,8-Dioxo-Octahydroxanthenes Employing Iron Oxide Nanomaterials Rajabi, Fatemeh Abdollahi, Mohammad Diarjani, Elham Sadat Osmolowsky, Mikhail G. Osmolovskaya, Olga M. Gómez-López, Paulette Puente-Santiago, Alain R. Luque, Rafael Materials (Basel) Article In this study, 1,8-dioxo-octahydroxanthenes were prepared employing a simple, effective and environmentally sound approach utilizing an iron oxide nanocatalyst under solventless conditions. The proposed iron oxide nanomaterial exhibited high product yields, short reaction times and a facile work-up procedure. The synthesized catalyst was also found to be highly stable and reusable under the investigated conditions (up to twelve consecutive cycles) without any significant loss in its catalytic activity. MDPI 2019-07-26 /pmc/articles/PMC6695819/ /pubmed/31357446 http://dx.doi.org/10.3390/ma12152386 Text en © 2019 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/).
spellingShingle Article
Rajabi, Fatemeh
Abdollahi, Mohammad
Diarjani, Elham Sadat
Osmolowsky, Mikhail G.
Osmolovskaya, Olga M.
Gómez-López, Paulette
Puente-Santiago, Alain R.
Luque, Rafael
Solvent-Free Preparation of 1,8-Dioxo-Octahydroxanthenes Employing Iron Oxide Nanomaterials
title Solvent-Free Preparation of 1,8-Dioxo-Octahydroxanthenes Employing Iron Oxide Nanomaterials
title_full Solvent-Free Preparation of 1,8-Dioxo-Octahydroxanthenes Employing Iron Oxide Nanomaterials
title_fullStr Solvent-Free Preparation of 1,8-Dioxo-Octahydroxanthenes Employing Iron Oxide Nanomaterials
title_full_unstemmed Solvent-Free Preparation of 1,8-Dioxo-Octahydroxanthenes Employing Iron Oxide Nanomaterials
title_short Solvent-Free Preparation of 1,8-Dioxo-Octahydroxanthenes Employing Iron Oxide Nanomaterials
title_sort solvent-free preparation of 1,8-dioxo-octahydroxanthenes employing iron oxide nanomaterials
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6695819/
https://www.ncbi.nlm.nih.gov/pubmed/31357446
http://dx.doi.org/10.3390/ma12152386
work_keys_str_mv AT rajabifatemeh solventfreepreparationof18dioxooctahydroxanthenesemployingironoxidenanomaterials
AT abdollahimohammad solventfreepreparationof18dioxooctahydroxanthenesemployingironoxidenanomaterials
AT diarjanielhamsadat solventfreepreparationof18dioxooctahydroxanthenesemployingironoxidenanomaterials
AT osmolowskymikhailg solventfreepreparationof18dioxooctahydroxanthenesemployingironoxidenanomaterials
AT osmolovskayaolgam solventfreepreparationof18dioxooctahydroxanthenesemployingironoxidenanomaterials
AT gomezlopezpaulette solventfreepreparationof18dioxooctahydroxanthenesemployingironoxidenanomaterials
AT puentesantiagoalainr solventfreepreparationof18dioxooctahydroxanthenesemployingironoxidenanomaterials
AT luquerafael solventfreepreparationof18dioxooctahydroxanthenesemployingironoxidenanomaterials