Resolution Enhancement in SEA XLOC for Heteronuclear NMR Long‐Range Correlation

It is shown how the resolution in SEA XLOC NMR spectra for distinguishing between heteronuclear two‐ and three‐bond correlations for all (13)C multiplicities can be improved by a modified experiment delivering absorptive profiles in the indirect dimension. The method is demonstrated with application...

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Detalles Bibliográficos
Autores principales: Gyöngyösi, Tamás, Kövér, Katalin E., Sørensen, Ole W.
Formato: Online Artículo Texto
Lenguaje:English
Publicado: John Wiley and Sons Inc. 2019
Materias:
Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6709521/
https://www.ncbi.nlm.nih.gov/pubmed/31463169
http://dx.doi.org/10.1002/open.201900136
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author Gyöngyösi, Tamás
Kövér, Katalin E.
Sørensen, Ole W.
author_facet Gyöngyösi, Tamás
Kövér, Katalin E.
Sørensen, Ole W.
author_sort Gyöngyösi, Tamás
collection PubMed
description It is shown how the resolution in SEA XLOC NMR spectra for distinguishing between heteronuclear two‐ and three‐bond correlations for all (13)C multiplicities can be improved by a modified experiment delivering absorptive profiles in the indirect dimension. The method is demonstrated with applications to ibuprofen and strychnine.
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spelling pubmed-67095212019-08-28 Resolution Enhancement in SEA XLOC for Heteronuclear NMR Long‐Range Correlation Gyöngyösi, Tamás Kövér, Katalin E. Sørensen, Ole W. ChemistryOpen Communications It is shown how the resolution in SEA XLOC NMR spectra for distinguishing between heteronuclear two‐ and three‐bond correlations for all (13)C multiplicities can be improved by a modified experiment delivering absorptive profiles in the indirect dimension. The method is demonstrated with applications to ibuprofen and strychnine. John Wiley and Sons Inc. 2019-06-26 /pmc/articles/PMC6709521/ /pubmed/31463169 http://dx.doi.org/10.1002/open.201900136 Text en ©2019 The Authors. Published by Wiley-VCH Verlag GmbH & Co. KGaA. This is an open access article under the terms of the http://creativecommons.org/licenses/by-nc-nd/4.0/ License, which permits use and distribution in any medium, provided the original work is properly cited, the use is non‐commercial and no modifications or adaptations are made.
spellingShingle Communications
Gyöngyösi, Tamás
Kövér, Katalin E.
Sørensen, Ole W.
Resolution Enhancement in SEA XLOC for Heteronuclear NMR Long‐Range Correlation
title Resolution Enhancement in SEA XLOC for Heteronuclear NMR Long‐Range Correlation
title_full Resolution Enhancement in SEA XLOC for Heteronuclear NMR Long‐Range Correlation
title_fullStr Resolution Enhancement in SEA XLOC for Heteronuclear NMR Long‐Range Correlation
title_full_unstemmed Resolution Enhancement in SEA XLOC for Heteronuclear NMR Long‐Range Correlation
title_short Resolution Enhancement in SEA XLOC for Heteronuclear NMR Long‐Range Correlation
title_sort resolution enhancement in sea xloc for heteronuclear nmr long‐range correlation
topic Communications
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6709521/
https://www.ncbi.nlm.nih.gov/pubmed/31463169
http://dx.doi.org/10.1002/open.201900136
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AT koverkataline resolutionenhancementinseaxlocforheteronuclearnmrlongrangecorrelation
AT sørensenolew resolutionenhancementinseaxlocforheteronuclearnmrlongrangecorrelation

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