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Effect on the characterization of metolachlor polyurea microcapsules with urea instead of polyamines

In this paper, a novel metolachlor microcapsules suspension (CS) was prepared by interfacial polymerization. Metolachlor polyurea microcapsules suspension was successfully prepared by urea instead of polyamines which could reduce the use of organic solvents and production costs. The synthesized micr...

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Detalles Bibliográficos
Autores principales: Li, Deming, Wang, Yan, Wang, Jun, Liu, Huanhuan
Formato: Online Artículo Texto
Lenguaje:English
Publicado: Taylor & Francis 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6713152/
https://www.ncbi.nlm.nih.gov/pubmed/31488960
http://dx.doi.org/10.1080/15685551.2019.1653031
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author Li, Deming
Wang, Yan
Wang, Jun
Liu, Huanhuan
author_facet Li, Deming
Wang, Yan
Wang, Jun
Liu, Huanhuan
author_sort Li, Deming
collection PubMed
description In this paper, a novel metolachlor microcapsules suspension (CS) was prepared by interfacial polymerization. Metolachlor polyurea microcapsules suspension was successfully prepared by urea instead of polyamines which could reduce the use of organic solvents and production costs. The synthesized microcapsules were characterized by Fourier Transform Infrared Spectrometer, Scanning Electron Microscope, Ultraviolet Spectrometry, Thermogravimetric analyses and particle size analyzer. In conclusion, the diameter of the urea microcapsules were the smallest (11.52 μm) and excellent encapsulation efficiency (81.45%). In addition, Urea microcapsules had compact microstructures and global shapes, which had a good thermal stability and metolachlor could be preserved better in the polyurea microcapsules. These results indicated that the prepared microcapsules by urea had better thermal storage properties and physicochemical property. The microcapsule suspension of metolachlor hasn’t been researched yet. Therefore, it is significant to prepare microcapsule suspension. More importantly, there is no use of organic solvents in the preparation of microcapsules suspension, which avoided the pollution of solvents to the ecological environment. It is hoped that this polyurea material will be applied in the field of pesticide synthesis and polymers.
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spelling pubmed-67131522019-09-05 Effect on the characterization of metolachlor polyurea microcapsules with urea instead of polyamines Li, Deming Wang, Yan Wang, Jun Liu, Huanhuan Des Monomers Polym Article In this paper, a novel metolachlor microcapsules suspension (CS) was prepared by interfacial polymerization. Metolachlor polyurea microcapsules suspension was successfully prepared by urea instead of polyamines which could reduce the use of organic solvents and production costs. The synthesized microcapsules were characterized by Fourier Transform Infrared Spectrometer, Scanning Electron Microscope, Ultraviolet Spectrometry, Thermogravimetric analyses and particle size analyzer. In conclusion, the diameter of the urea microcapsules were the smallest (11.52 μm) and excellent encapsulation efficiency (81.45%). In addition, Urea microcapsules had compact microstructures and global shapes, which had a good thermal stability and metolachlor could be preserved better in the polyurea microcapsules. These results indicated that the prepared microcapsules by urea had better thermal storage properties and physicochemical property. The microcapsule suspension of metolachlor hasn’t been researched yet. Therefore, it is significant to prepare microcapsule suspension. More importantly, there is no use of organic solvents in the preparation of microcapsules suspension, which avoided the pollution of solvents to the ecological environment. It is hoped that this polyurea material will be applied in the field of pesticide synthesis and polymers. Taylor & Francis 2019-08-17 /pmc/articles/PMC6713152/ /pubmed/31488960 http://dx.doi.org/10.1080/15685551.2019.1653031 Text en © 2019 The Author(s). Published by Informa UK Limited, trading as Taylor & Francis Group. http://creativecommons.org/licenses/by/4.0/ This is an Open Access article distributed under the terms of the Creative Commons Attribution License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution, and reproduction in any medium, provided the original work is properly cited.
spellingShingle Article
Li, Deming
Wang, Yan
Wang, Jun
Liu, Huanhuan
Effect on the characterization of metolachlor polyurea microcapsules with urea instead of polyamines
title Effect on the characterization of metolachlor polyurea microcapsules with urea instead of polyamines
title_full Effect on the characterization of metolachlor polyurea microcapsules with urea instead of polyamines
title_fullStr Effect on the characterization of metolachlor polyurea microcapsules with urea instead of polyamines
title_full_unstemmed Effect on the characterization of metolachlor polyurea microcapsules with urea instead of polyamines
title_short Effect on the characterization of metolachlor polyurea microcapsules with urea instead of polyamines
title_sort effect on the characterization of metolachlor polyurea microcapsules with urea instead of polyamines
topic Article
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6713152/
https://www.ncbi.nlm.nih.gov/pubmed/31488960
http://dx.doi.org/10.1080/15685551.2019.1653031
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