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The Effects of Sintering Temperature and Addition of TiH(2) on the Sintering Process of Cu

In this study, effects of sintering temperature and TiH(2) on the sintering process of Cu are investigated. During sintering, the oxide in Cu decomposes and generates oxygen, which can become trapped in the material forming closed pores. Therefore, this results in low sintered density. Sintering beh...

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Detalles Bibliográficos
Autores principales: Hao, Huali, Wang, Yanjing, Jafari Nodooshan, Hamid Reza, Zhang, Yongyun, Ye, Shulong, Lv, Yonghu, Yu, Peng
Formato: Online Artículo Texto
Lenguaje:English
Publicado: MDPI 2019
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6721083/
https://www.ncbi.nlm.nih.gov/pubmed/31443144
http://dx.doi.org/10.3390/ma12162594
Descripción
Sumario:In this study, effects of sintering temperature and TiH(2) on the sintering process of Cu are investigated. During sintering, the oxide in Cu decomposes and generates oxygen, which can become trapped in the material forming closed pores. Therefore, this results in low sintered density. Sintering behavior of Cu can be significantly improved by adding 0.5 wt.% TiH(2) which decomposes during sintering, producing hydrogen and effectively reducing the oxide in Cu. Although gas products of the reduction reaction may still be trapped inside the close pores formed near the TiH(2) particles and handicap the sintering of Cu, an isothermal treatment at 650 °C can avoid forming close pores. This allows reaction products to dissipate freely from the sample, subsequently increasing its sintered density.