Crystal structure and chemistry of tricadmium digermanium tetra­arsenide, Cd(3)Ge(2)As(4)

A cadmium germanium arsenide compound, Cd(3)Ge(2)As(4), was synthesized using a double-containment fused quartz ampoule method within a rocking furnace and a melt-quench technique. The crystal structure was determined from single-crystal X-ray diffraction (SC-XRD), scanning and transmission electron...

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Detalles Bibliográficos
Autores principales: Thompson, Michael R., Riley, Brian J., Bowden, Mark E., Olszta, Matthew J., Edwards, Danny J., Crum, Jarrod V., Johnson, Bradley R., Chong, Saehwa
Formato: Online Artículo Texto
Lenguaje:English
Publicado: International Union of Crystallography 2019
Materias:
Research Communications
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6727045/
https://www.ncbi.nlm.nih.gov/pubmed/31523452
http://dx.doi.org/10.1107/S2056989019010636
Descripción
Sumario:A cadmium germanium arsenide compound, Cd(3)Ge(2)As(4), was synthesized using a double-containment fused quartz ampoule method within a rocking furnace and a melt-quench technique. The crystal structure was determined from single-crystal X-ray diffraction (SC-XRD), scanning and transmission electron microscopies (i.e. SEM, STEM, and TEM), and selected area diffraction (SAD) and confirmed with electron backscatter diffraction (EBSD). The chemistry was verified with electron energy loss spectroscopy (EELS).

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