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Urea assisted ceria nanocubes for efficient removal of malachite green organic dye from aqueous system
This study describes a simple, high-yield, rapid, and inexpensive route for the synthesis of cubic shape-like cerium oxide nanocubes (CeO(2) NCs) using different urea concentrations (0.5, 1.0, and 2.0 g) by the hydrothermal method. The synthesized nanocubes (NCs) are labeled as CeO(2) NCs-0.5, CeO(2...
Autores principales: | , , , , |
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Formato: | Online Artículo Texto |
Lenguaje: | English |
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Nature Publishing Group UK
2019
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6785541/ https://www.ncbi.nlm.nih.gov/pubmed/31597923 http://dx.doi.org/10.1038/s41598-019-50984-6 |
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author | Sreekanth, Thupakula Venkata Madhukar Nagajyothi, Patnamsetty Chidanandha Reddy, Gutturu Rajasekhara Shim, Jaesool Yoo, Kisoo |
author_facet | Sreekanth, Thupakula Venkata Madhukar Nagajyothi, Patnamsetty Chidanandha Reddy, Gutturu Rajasekhara Shim, Jaesool Yoo, Kisoo |
author_sort | Sreekanth, Thupakula Venkata Madhukar |
collection | PubMed |
description | This study describes a simple, high-yield, rapid, and inexpensive route for the synthesis of cubic shape-like cerium oxide nanocubes (CeO(2) NCs) using different urea concentrations (0.5, 1.0, and 2.0 g) by the hydrothermal method. The synthesized nanocubes (NCs) are labeled as CeO(2) NCs-0.5, CeO(2) NCs-1.0, and CeO(2) NCs-2.0, corresponding to 0.5, 1.0, and 2.0 g of urea, respectively. The synthesized NCs were characterized by FT-IR, UV-visible, XRD, XPS, SEM and HR-TEM analysis. The synthesized NCs were cubic in shape with average sizes of 12, 12, and 13 nm for the CeO(2) NCs-0.5, CeO(2) NCs-1.0, and CeO(2) NCs-2.0, respectively, obtained by the XRD analysis. The catalytic activity of the CeO(2) NCs was studied for the purpose of obtaining the reduction of malachite green (MG) in the presence of sodium borohydride (NaBH(4)) at room temperature. |
format | Online Article Text |
id | pubmed-6785541 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2019 |
publisher | Nature Publishing Group UK |
record_format | MEDLINE/PubMed |
spelling | pubmed-67855412019-10-17 Urea assisted ceria nanocubes for efficient removal of malachite green organic dye from aqueous system Sreekanth, Thupakula Venkata Madhukar Nagajyothi, Patnamsetty Chidanandha Reddy, Gutturu Rajasekhara Shim, Jaesool Yoo, Kisoo Sci Rep Article This study describes a simple, high-yield, rapid, and inexpensive route for the synthesis of cubic shape-like cerium oxide nanocubes (CeO(2) NCs) using different urea concentrations (0.5, 1.0, and 2.0 g) by the hydrothermal method. The synthesized nanocubes (NCs) are labeled as CeO(2) NCs-0.5, CeO(2) NCs-1.0, and CeO(2) NCs-2.0, corresponding to 0.5, 1.0, and 2.0 g of urea, respectively. The synthesized NCs were characterized by FT-IR, UV-visible, XRD, XPS, SEM and HR-TEM analysis. The synthesized NCs were cubic in shape with average sizes of 12, 12, and 13 nm for the CeO(2) NCs-0.5, CeO(2) NCs-1.0, and CeO(2) NCs-2.0, respectively, obtained by the XRD analysis. The catalytic activity of the CeO(2) NCs was studied for the purpose of obtaining the reduction of malachite green (MG) in the presence of sodium borohydride (NaBH(4)) at room temperature. Nature Publishing Group UK 2019-10-09 /pmc/articles/PMC6785541/ /pubmed/31597923 http://dx.doi.org/10.1038/s41598-019-50984-6 Text en © The Author(s) 2019 Open Access This article is licensed under a Creative Commons Attribution 4.0 International License, which permits use, sharing, adaptation, distribution and reproduction in any medium or format, as long as you give appropriate credit to the original author(s) and the source, provide a link to the Creative Commons license, and indicate if changes were made. The images or other third party material in this article are included in the article’s Creative Commons license, unless indicated otherwise in a credit line to the material. If material is not included in the article’s Creative Commons license and your intended use is not permitted by statutory regulation or exceeds the permitted use, you will need to obtain permission directly from the copyright holder. To view a copy of this license, visit http://creativecommons.org/licenses/by/4.0/. |
spellingShingle | Article Sreekanth, Thupakula Venkata Madhukar Nagajyothi, Patnamsetty Chidanandha Reddy, Gutturu Rajasekhara Shim, Jaesool Yoo, Kisoo Urea assisted ceria nanocubes for efficient removal of malachite green organic dye from aqueous system |
title | Urea assisted ceria nanocubes for efficient removal of malachite green organic dye from aqueous system |
title_full | Urea assisted ceria nanocubes for efficient removal of malachite green organic dye from aqueous system |
title_fullStr | Urea assisted ceria nanocubes for efficient removal of malachite green organic dye from aqueous system |
title_full_unstemmed | Urea assisted ceria nanocubes for efficient removal of malachite green organic dye from aqueous system |
title_short | Urea assisted ceria nanocubes for efficient removal of malachite green organic dye from aqueous system |
title_sort | urea assisted ceria nanocubes for efficient removal of malachite green organic dye from aqueous system |
topic | Article |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC6785541/ https://www.ncbi.nlm.nih.gov/pubmed/31597923 http://dx.doi.org/10.1038/s41598-019-50984-6 |
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